5-甲基-2-苯基-4,5-二氢-1,3-噻唑合成路线 （共 10 条）
反应条件
nonafluoro-n-butanesulfonyl fluoride; triethylamine in dichloromethane
T=20°C;
参考文献
Yan, Zhaohua; Guan, Chengbo; Yu, Zhangxin; Tian, Weisheng
Tetrahedron Letters, 2013 , vol. 54, # 43 p. 5788 - 5790
反应条件
toluene-4-sulfonic acid in toluene
23 h; Heating;
参考文献
Engman, Lars
Journal of Organic Chemistry, 1991 , vol. 56, # 10 p. 3425 - 3430
反应条件
1: 85 percent / Lawesson's reagent / tetrahydrofuran / Heating
2: 85 percent / CHCl3 / 3 h
3: 91 percent / Ph3SnH / 1 h
View Scheme
参考文献
Engman, Lars
Journal of Organic Chemistry, 1991 , vol. 56, # 10 p. 3425 - 3430
反应条件
triphenylstannane
1 h;
参考文献
Engman, Lars
Journal of Organic Chemistry, 1991 , vol. 56, # 10 p. 3425 - 3430
反应条件
Lawesson's reagent in toluene
Heating;
参考文献
Nishio, Takehiko
Journal of Organic Chemistry, 1997 , vol. 62, # 4 p. 1106 - 1111
反应条件
1: 40 percent / S / dioxane / 3 h / Heating
2: 1.) P4S10; 2.) Na2CO3 / 1.) 150 deg C; 2.) reflux, 2 h
View Scheme
参考文献
Robbe; Fernandez; Chapat; et al.
European Journal of Medicinal Chemistry, 1985 , vol. 20, # 1 p. 16 - 24
反应条件
1: P2S5 / pyridine / 0.75 h / Heating
2: 18 percent / methanol / 15 h / Irradiation
View Scheme
参考文献
Couture, A.; Dubiez, R.; Lablanche-Combier, A.
Tetrahedron, 1984 , vol. 40, # 10 p. 1835 - 1844
反应条件
diphosphorus pentasulfide
T=150°C;
参考文献
Salomon
Chemische Berichte, 1893 , vol. 26, p. 1322
参考文献
Gabriel; v. Hirsch
Chemische Berichte, 1896 , vol. 29, p. 2610
参考文献
Gabriel; Heymann
Chemische Berichte, 1891 , vol. 24, p. 784
