N-(2-羟基丙基)苯甲酰胺合成路线 （共 18 条）
反应条件
triethylamine in dichloromethane
参考文献
Bigge, Christopher Franklin; Bridges, Alexander James; Casimiro-Garcia, Agustin; Fakhoury, Stephen Alan; Lee, Helen Tsenwhei; Reed, Jessica; Schaum, Robert; Schlosser, Kevin Matthew; Sexton, Karen; Zhou, Hairong
Patent: US2003/171377 A1, 2003 ;
反应条件
triethylamine in dichloromethane
参考文献
Bigge, Christopher Franklin; Bridges, Alexander James; Casimiro-Garcia, Agustin; Fakhoury, Stephen Alan; Lee, Helen Tsenwhei; Reed, Jessica; Schaum, Robert; Schlosser, Kevin Matthew; Sexton, Karen; Zhou, Hairong
Patent: US2003/171377 A1, 2003 ;
反应条件
oxygen; cobalt(II) 2,4-pentanedionate in isopropyl alcohol T=75°C; 1 h;
参考文献
Kato; Yamada; Takai; Inoki; Isayama
Bulletin of the Chemical Society of Japan, 1990 , vol. 63, # 1 p. 179 - 186
反应条件
hydrogen fluoride; SbF5 T=-20°C; 0.166667 h;
参考文献
Thibaudeau, Sebastien; Martin-Mingot, Agnes; Jouannetaud, Marie-Paule; Karam, Omar; Zunino, Fabien
Chemical Communications, 2007 , # 30 p. 3198 - 3200
反应条件
bis(cyclopentadienyl)titanium dichloride in tetrahydrofuran T=25°C; 18 h;
参考文献
Yokomatsu, Tsutomu; Arakawa, Akio; Shibuya, Shiroshi
Journal of Organic Chemistry, 1994 , vol. 59, # 12 p. 3506 - 3508
反应条件
oxygen; isopropyl alcohol; bis(trifluoroacetylacetonato)cobalt(II) T=75°C; 4 h;
参考文献
Isayama, Shigeru; Mukaiyama, Teruaki
Chemistry Letters, 1989 , p. 569 - 572
反应条件
1: DMAP / tetrahydrofuran / 18 h / Ambient temperature 2: Cp2TiCl2 / tetrahydrofuran / 18 h / Ambient temperature 3: 65 percent / NaNO2, H2SO4 / aq. acetic acid / 1.) r.t., 18 h, 2.) 50 deg C, 15 min View Scheme
参考文献
Hirsch
Chemische Berichte, 1890 , vol. 23, p. 968
反应条件
1: Cp2TiCl2 / tetrahydrofuran / 18 h / Ambient temperature 2: 65 percent / NaNO2, H2SO4 / aq. acetic acid / 1.) r.t., 18 h, 2.) 50 deg C, 15 min View Scheme
参考文献
Yokomatsu, Tsutomu; Arakawa, Akio; Shibuya, Shiroshi
Journal of Organic Chemistry, 1994 , vol. 59, # 12 p. 3506 - 3508
反应条件
N(Et)4ClO4 in acetonitrile T=23°C;
参考文献
Arai, Kenji; Tamura, Shohei; Masumizu, Tatsuya; Kawai, Ken-Ichi; Nakajima, Shoichi; Ueda, Akira
Canadian Journal of Chemistry, 1990 , vol. 68, # 6 p. 903 - 907
反应条件
in dichloromethane 15 h; Ambient temperature;
参考文献
Murahashi; Naota
Synthesis, 1993 , # 4 p. 433 - 440
