3-苯基-1-氨基异喹啉合成路线 （共 25 条）
反应条件
hydrogen; palladium on activated charcoal in acetic acid
T=66°C; P=4654.33 Torr;
参考文献
Cho, Won-Jea; Kim, Eui-Ki; Park, Il Yeong; Jeong, Eun Young; Kim, Tae Sung; Le, Thanh Nguyen; Kim, Dae-Duk; Lee, Eung-Seok
Bioorganic and Medicinal Chemistry, 2002 , vol. 10, # 9 p. 2953 - 2961
反应条件
silver hexafluoroantimonate; NaAuCl4*2H2O; ammonium acetate in acetonitrile
T=85°C; 20 h;
参考文献
Long, Yuhua; She, Zhigang; Liu, Xiaochen; Chen, Yu
Journal of Organic Chemistry, 2013 , vol. 78, # 6 p. 2579 - 2588
反应条件
silver hexafluoroantimonate; NaAuCl4*2H2O; ammonium acetate in acetonitrile
T=85°C; 20 h;
参考文献
Long, Yuhua; She, Zhigang; Liu, Xiaochen; Chen, Yu
Journal of Organic Chemistry, 2013 , vol. 78, # 6 p. 2579 - 2588
反应条件
1: POCl3
2: K2CO3 / dimethylformamide / Heating
3: H2 / Pd/C / acetic acid / 4137.18 Torr
View Scheme
参考文献
Cho, Won-Jea; Min, Sun Young; Le, Thanh Nguyen; Kim, Tae Sung
Bioorganic and Medicinal Chemistry Letters, 2003 , vol. 13, # 24 p. 4451 - 4454
反应条件
1: n-BuLi / tetrahydrofuran
2: POCl3
3: K2CO3 / dimethylformamide / Heating
4: H2 / Pd/C / acetic acid / 4137.18 Torr
View Scheme
参考文献
Cho, Won-Jea; Min, Sun Young; Le, Thanh Nguyen; Kim, Tae Sung
Bioorganic and Medicinal Chemistry Letters, 2003 , vol. 13, # 24 p. 4451 - 4454
反应条件
1: n-BuLi / tetrahydrofuran
2: POCl3
3: K2CO3 / dimethylformamide / Heating
4: H2 / Pd/C / acetic acid / 4137.18 Torr
View Scheme
参考文献
Cho, Won-Jea; Min, Sun Young; Le, Thanh Nguyen; Kim, Tae Sung
Bioorganic and Medicinal Chemistry Letters, 2003 , vol. 13, # 24 p. 4451 - 4454
反应条件
silver hexafluoroantimonate; NaAuCl4*2H2O; ammonium acetate in acetonitrile
T=85°C; 20 h;
参考文献
Long, Yuhua; She, Zhigang; Liu, Xiaochen; Chen, Yu
Journal of Organic Chemistry, 2013 , vol. 78, # 6 p. 2579 - 2588
反应条件
silver hexafluoroantimonate; NaAuCl4*2H2O; ammonium acetate in acetonitrile
T=85°C; 20 h;
参考文献
Long, Yuhua; She, Zhigang; Liu, Xiaochen; Chen, Yu
Journal of Organic Chemistry, 2013 , vol. 78, # 6 p. 2579 - 2588
反应条件
1: 87 percent Spectr. / (PPh3)2PdCl2; CuI; DIPA / tetrahydrofuran
2: 63 percent / CH2Cl2 / 1 h / 20 °C
3: 32 percent / NH3 / CH2Cl2 / 20 h
View Scheme
参考文献
Tovar, John D.; Swager, Timothy M.
Journal of Organic Chemistry, 1999 , vol. 64, # 17 p. 6499 - 6504
反应条件
1: 63 percent / CH2Cl2 / 1 h / 20 °C
2: 32 percent / NH3 / CH2Cl2 / 20 h
View Scheme
参考文献
Tovar, John D.; Swager, Timothy M.
Journal of Organic Chemistry, 1999 , vol. 64, # 17 p. 6499 - 6504
