3-吗啉基-1-苯基丙酮合成路线 (共 20 条)
反应条件
sodium tris(acetoxy)borohydride in 1,4-dioxane T=20°C; 10 h;
参考文献
Ueno, Satoshi; Shimizu, Ryosuke; Kuwano, Ryoichi
Angewandte Chemie, International Edition, 2009 , vol. 48, p. 4543 - 4545
Angewandte Chemie, 2009 , vol. 121, p. 4613 - 4615
反应条件
1: bromobenzene With magnesium in tetrahydrofuran 1 h; Heating; 2: N-methoxy-N-methyl-3-morpholin-4-yl-propionamide in tetrahydrofuran T=0°C;
参考文献
Selvamurugan; Aidhen
Synthesis, 2001 , # 15 p. 2239 - 2246
反应条件
hydrogenchloride in ethanol 6 h; Heating;
参考文献
Sharma. V. L.; Bhandari, Kalpana; Chatterjee, S. K.; Satyanarayana, K. V.; Dua, P. R.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1994 , vol. 33, # 4 p. 393 - 396
反应条件
1: With hydrogenchloride in propan-1-ol; water Mannich Aminomethylation; 2: With sodium hydrogencarbonate in propan-1-ol; water
参考文献
Bishnoi, Abha; Singh, Suruchi; Tiwari, Anil K.; Rani, Archna; Jain, Sapna; Tripathic
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2014 , vol. 53, # 3 p. 325 - 331
反应条件
acetic acid in acetonitrile Mannich reaction; 14 h; Reflux;
参考文献
Guo, Yuan; An, Jing; Lu, Zhenhuan; Peng, Mengjiao
Chinese Journal of Chemistry, 2012 , vol. 30, # 7 p. 1561 - 1564
反应条件
diethyl ether anschliessend Behandeln mit wss. HCl;
参考文献
Journal of the American Chemical Society, 77 <1955< 2817
参考文献
Journal of the American Chemical Society, , vol. 74, p. 3875
Journal of the American Pharmaceutical Association (1912-1977), , vol. 47, p. 77,80
反应条件
1: NaI / acetone 2: acetonitrile / 25 °C View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 22, # 10 p. 1918 - 1921
Zhurnal Organicheskoi Khimii, , vol. 22, # 10 p. 2138 - 2142
参考文献
Journal of the American Chemical Society, , vol. 70, p. 4230
Journal of the Chemical Society, , p. 1039,1043
Journal and Proceedings of the Royal Society of New South Wales, , vol. 72, p. 239
Chem. Zentralbl., , vol. 110, # I p. 1959
参考文献
Journal of the American Chemical Society, , vol. 70, p. 4230
Yakugaku Zasshi, , vol. 76, p. 1
Chem.Abstr., , p. 13029