1: NaBH4 / methanol / Ambient temperature 2: toluene-p-sulfonic acid / toluene / 4 h / Heating 3: 96 percent / diisobutylaluminium hydride / diethyl ether; hexane / 1) -78 deg C to room temperature, 2) room temperature, 8 h View Scheme
参考文献
Murphy, John A.; Patterson, Christopher W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 4 p. 405 - 410
potassium tert-butylate in tetrahydrofuran 1 h; Ambient temperaturein the presence or absence of various radical inhibitors, different iodonium salts; Product distributionMechanism;
参考文献
Journal of Organic Chemistry, , vol. 62, # 7 p. 2130 - 2138