3-(2-噻吩基)-L-丙氨酸合成路线 (共 17 条)
反应条件
ammonium hydroxide; carbon dioxide; phenylalanine ammonia-lyase T=30°C; pH=10.2; 48 h;
参考文献
Paizs, Csaba; Katona, Adrian; Retey, Janos
Chemistry - A European Journal, 2006 , vol. 12, # 10 p. 2739 - 2744
反应条件
1: 97 percent / 2 N aq. NaOH / dioxane / 4 h / 50 °C 3: 90 percent / trifluoroacetic acid / 0.33 h View Scheme
参考文献
Polish Journal of Chemistry, , vol. 54, # 11/12 p. 2225 - 2228
反应条件
trifluoroacetic acid 0.333333 h;
参考文献
Lipkowski, Andrzej W.; Flouret, George
Polish Journal of Chemistry, 1980 , vol. 54, # 11/12 p. 2225 - 2228
反应条件
1: 88 percent / NaOAc, Ac2O / 1.5 h / Heating 2: 94 percent / HCl (gas), H2O / dioxane 3: aq. HCl / Heating 4: 57 percent / L-aspartic acid, pyridoxal phosphate, E. coli strain, aq. NaOH View Scheme
参考文献
Tetrahedron: Asymmetry, , vol. 8, # 4 p. 527 - 536
反应条件
1: 94 percent / HCl (gas), H2O / dioxane 2: aq. HCl / Heating 3: 57 percent / L-aspartic acid, pyridoxal phosphate, E. coli strain, aq. NaOH View Scheme
参考文献
Tetrahedron: Asymmetry, , vol. 8, # 4 p. 527 - 536
反应条件
ammonium hydroxide; anhydrous cobalt diacetate; trifluoroacetic acid 1) acylase I, H2O, 38 deg C, 2) 50 deg C, 10 min; Yield given. Multistep reaction;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 4 p. 1151 - 1158
参考文献
Journal of Biological Chemistry, , vol. 174, p. 241,242
反应条件
carboxypeptidase-substance from bovine pancreas
参考文献
Journal of Organic Chemistry, , vol. 15, p. 688,691, 693
反应条件
1: aq. HCl / Heating 2: 57 percent / L-aspartic acid, pyridoxal phosphate, E. coli strain, aq. NaOH View Scheme
参考文献
Tetrahedron: Asymmetry, , vol. 8, # 4 p. 527 - 536
反应条件
1: 5N aq. NaOH / 1 h / Heating 2: 57 percent / L-aspartic acid, pyridoxal phosphate, E. coli strain, aq. NaOH View Scheme
参考文献
Tetrahedron: Asymmetry, , vol. 8, # 4 p. 527 - 536