1-溴-4-丙-2-烯基苯合成路线 （共 25 条）
反应条件
1: p-bromophenyl bromide With magnesium in tetrahydrofuran Heating; 2: allyl bromide in tetrahydrofuran Heating;
参考文献
Mueller, Jan; Brunnbauer, Markus; Schmidt, Michael; Zimmermann, Anja; Terfort, Andreas
Synthesis, 2005 , # 6 art. no. T10004SS, p. 998 - 1004
参考文献
Nycomed Imaging AS
Patent: US6284894 B1, 2001 ;
反应条件
bis(η3-allyl-μ-chloropalladium(II)) in diethyl ether; benzene 3 h;
参考文献
Kasatkin, A. N.; Kulak, A. N.; Tolstikov, G. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1987 , vol. 36, # 2 p. 350 - 355
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1987 , # 2 p. 391 - 396
反应条件
bis(η3-allyl-μ-chloropalladium(II)) in diethyl ether; benzene reaction of soln. of p-BrC6H4Ti(i-OPr)3 in ether (obtained from reaction of p-BrC6H4MgBr with ClTi(i-OPr)3 in ether) with soln. of bromide and (C3H5PdCl)2 in benzene at 20°C under Ar;; not isolated;;
参考文献
Kasatkin, A. N.; Kulak, A. N.; Tolstikov, G. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1987 , vol. 36, # 2 p. 350 - 355
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1987 , # 2 p. 391 - 396
反应条件
bis(acetylacetonate)nickel(II); diethylzinc 1.) THF, rt, 6 h, 2.) THF, -60 deg C to rt; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Stuedemann, Thomas; Gupta, Vijay; Engman, Lars; Knochel, Paul
Tetrahedron Letters, 1997 , vol. 38, # 6 p. 1005 - 1008
参考文献
Liberman,A.L. et al.
Doklady Chemistry, 1960 , vol. 134, p. 1051 - 1054
Doklady Akademii Nauk SSSR, 1960 , vol. 134, p. 603 - 606
参考文献
Quelet
Bulletin de la Societe Chimique de France, 1929 , vol. <4> 45, p. 78
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1926 , vol. 182, p. 1284
反应条件
1: toluene / 1 h / 60 °C / Inert atmosphere; Sealed tube 2: 1,10-phenanthroline; potassium tert-butylate; anhydrous copper acetate / toluene / 12 h / 100 °C / 760.05 Torr View Scheme
参考文献
Ohishi, Takeshi; Zhang, Liang; Nishiura, Masayoshi; Hou, Zhaomin
Angewandte Chemie - International Edition, 2011 , vol. 50, # 35 p. 8114 - 8117
反应条件
1: 1-allyl-4-bromobenzene With iron (III) acetylacetonate; 2,4,6-trimethylphenyl iodide; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in tetrahydrofuran T=20°C; 0.5 h; Inert atmosphere; 2: phenyl-magnesium bromide in tetrahydrofuran T=0°C; 0.5 h; Inert atmosphere;
参考文献
Organic Letters, , vol. 15, # 3 p. 714 - 717
反应条件
Behandeln des Reaktionsprodukts mit Wasser;
参考文献
Quelet
Bulletin de la Societe Chimique de France, 1929 , vol. <4> 45, p. 270
