甲基 7-甲氧基苯并[d][1,3]二氧代-5-羧酸合成路线 （共 32 条）
反应条件
thionyl chloride 3 h; Reflux;
参考文献
Semenov, Victor V.; Kiselyov, Alex S.; Titov, Ilia Y.; Sagamanova, Irina K.; Ikizalp, Natalie N.; Chernysheva, Natalia B.; Tsyganov, Dmitry V.; Konyushkin, Leonid D.; Firgang, Sergei I.; Semenov, Roman V.; Karmanova, Irina B.; Raihstat, Mikhail M.; Semenova, Marina N.
Journal of Natural Products, 2010 , vol. 73, # 11 p. 1796 - 1802
反应条件
1: potassium carbonate / dimethylformamide / 12 h / 70 °C 2: hydrochloric acid / methanol; H2O / 2 h / 20 °C 3: 85 percent / potassium fluoride / dimethylformamide / 110 °C View Scheme
参考文献
Tetrahedron, , vol. 61, # 7 p. 1909 - 1918
反应条件
1.1: pyridine; ozone / methanol; chloroform / -15 - 0 °C 2.1: ammonium hydroxide; iodine / tetrahydrofuran; water / 16 h / 20 °C 2.2: 4 h / Reflux 3.1: thionyl chloride / 3 h / Reflux View Scheme
参考文献
Journal of Natural Products, , vol. 73, # 11 p. 1796 - 1802
反应条件
1.1: tetrabutylammomium bromide; potassium hydroxide / 0.67 h / 100 °C 2.1: pyridine; ozone / methanol; chloroform / -15 - 0 °C 3.1: ammonium hydroxide; iodine / tetrahydrofuran; water / 16 h / 20 °C 3.2: 4 h / Reflux 4.1: thionyl chloride / 3 h / Reflux View Scheme
参考文献
Journal of Natural Products, , vol. 73, # 11 p. 1796 - 1802
反应条件
1: conc. H2SO4 / 6 h / Heating 2: 49.7 g / KF / dimethylformamide / 2.5 h / Heating View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 58, # 1 p. 346 - 351
反应条件
1.1: ammonium hydroxide; iodine / tetrahydrofuran; water / 16 h / 20 °C 1.2: 4 h / Reflux 2.1: thionyl chloride / 3 h / Reflux View Scheme
参考文献
Journal of Natural Products, , vol. 73, # 11 p. 1796 - 1802
反应条件
1: 42 percent / 50percent aq.potassium hydroxide / methanol / 9 h / Heating 2: diethyl ether View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 12 p. 2945 - 2947
反应条件
1: palladium 10 on activated carbon; hydrogen / ethanol 2: potassium carbonate / N,N-dimethyl-formamide View Scheme
反应条件
potassium carbonate in N,N-dimethyl-formamide 4 h; Heating;
参考文献
Zhang, Wei-Ge; Zhao, Rui; Ren, Jian; Ren, Li-Xiang; Lin, Jin-Guang; Liu, Dai-Lin; Wu, Ying-Liang; Yao, Xin-Sheng
Archiv der Pharmazie, 2007 , vol. 340, # 5 p. 244 - 250
参考文献
Austral. J. scient. Res., , vol. <A> 5, p. 412,418
