N-(2,4-二氯苯基)甲酰胺合成路线 （共 11 条）
参考文献
Das, Biswanath; Krishnaiah, Maddeboina; Balasubramanyam; Veeranjaneyulu, Boyapati; Nandan Kumar
Tetrahedron Letters, 2008 , vol. 49, # 14 p. 2225 - 2227
反应条件
in tetrahydrofuran T=60°C; 22.5 h;
参考文献
CONVERGENCE PHARMACEUTICALS LIMITED; BESWICK, Paul John; GLEAVE, Robert James; HACHISU, Shuji; VILE, Sadie; BERTHELEME, Nicolas; WARD, Simon E
Patent: WO2012/4604 A1, 2012 ;
Location in patent: Page/Page column 43 ;
WO 2012/004604 A1
反应条件
in tetrahydrofuran T=-20°C; 0.25 h;
参考文献
Krishnamurthy, S.
Tetrahedron Letters, 1982 , vol. 23, # 33 p. 3315 - 3318
反应条件
SCl2; chlorine Chlorierung mit oder ohne Loesungsmittel;
参考文献
Chattaway; Orton
Journal of the Chemical Society, 1899 , vol. 75, p. 1050
Journal of the Chemical Society, 1901 , vol. 79, p. 277
反应条件
1: potassium carbonate; calcium chloride 2: 200 - 210 °C View Scheme
参考文献
Chattaway; Orton
Journal of the Chemical Society, 1899 , vol. 75, p. 1050
Journal of the Chemical Society, 1901 , vol. 79, p. 277
反应条件
1: beim Aufbewahren 2: potassium carbonate; calcium chloride 3: 200 - 210 °C View Scheme
参考文献
Chattaway; Orton
Journal of the Chemical Society, 1899 , vol. 75, p. 1050
Journal of the Chemical Society, 1901 , vol. 79, p. 277
参考文献
Bly; Perkins; Lewis
Journal of the American Chemical Society, 1922 , vol. 44, p. 2900
参考文献
Bly; Perkins; Lewis
Journal of the American Chemical Society, 1922 , vol. 44, p. 2900
反应条件
T=70°C; reagiert 3 Mol Sulfurylchlorid;
参考文献
Meybeck
Annales de Chimie (Cachan, France), 1932 , vol. <10>7, p. 129,198
反应条件
dimethylsulfide borane complex in tetrahydrofuran 3 h; Heating; Yield given;
参考文献
Krishnamurthy, S.
Tetrahedron Letters, 1982 , vol. 23, # 33 p. 3315 - 3318
