2-(2-溴乙基)苯甲醛合成路线 （共 32 条）
反应条件
1: methanol; aq. NaOH solution; hydroxylamine 2: butan-1-ol; sodium View Scheme
参考文献
Schmitz
Chemische Berichte, 1958 , vol. 91, p. 1495,1502
反应条件
1: 80 percent / MeONa / methanol / 1 h / 0 °C 2: 53 percent / AcCl, FeCl3 / CH2Cl2 / 3 h / 0 - 5 °C 3: 95 percent / aq. NaH2PO2 / 10percent Pd-C / ethyl acetate / 0.58 h / Heating 4: 89 percent / ethanol; H2O / 24 h / Heating 5: 70 percent / aq. HCl / 2.5 h / Heating 6: 87 percent / pyridine / CH2Cl2 / 4 h / 5 - 10 °C View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 32, # 3 p. 875 - 882
反应条件
1: 80 percent / MeONa / methanol / 1 h / 0 °C 2: 53 percent / AcCl, FeCl3 / CH2Cl2 / 3 h / 0 - 5 °C View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 32, # 3 p. 875 - 882
反应条件
1: 80 percent / MeONa / methanol / 1 h / 0 °C 2: 53 percent / AcCl, FeCl3 / CH2Cl2 / 3 h / 0 - 5 °C 3: 95 percent / aq. NaH2PO2 / 10percent Pd-C / ethyl acetate / 0.58 h / Heating View Scheme
参考文献
Hayler; Howie; Giles; Negus; Oxley; Walsgrove; Walsh; Dagger; Fortunak; Mastrocola
Journal of Heterocyclic Chemistry, 1995 , vol. 32, # 3 p. 875 - 882
反应条件
1: 80 percent / MeONa / methanol / 1 h / 0 °C 2: 53 percent / AcCl, FeCl3 / CH2Cl2 / 3 h / 0 - 5 °C 3: 95 percent / aq. NaH2PO2 / 10percent Pd-C / ethyl acetate / 0.58 h / Heating 4: 89 percent / ethanol; H2O / 24 h / Heating 5: 70 percent / aq. HCl / 2.5 h / Heating View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 32, # 3 p. 875 - 882
反应条件
1: methanol; ammonia 2: diethyl ether; benzene View Scheme
参考文献
Schmitz
Chemische Berichte, 1958 , vol. 91, p. 1133,1138
反应条件
1: methanol; ammonia 2: tetrahydrofuran; benzene View Scheme
参考文献
Schmitz
Chemische Berichte, 1958 , vol. 91, p. 1133,1138
反应条件
methanol; sodium hydroxide; hydroxylamine
参考文献
Schmitz
Chemische Berichte, 1958 , vol. 91, p. 1495,1502
反应条件
in ethanol
T=0 - 20°C; Yield given;
参考文献
Page, Philip C. Bulman; Rassias, Gerasimos A.; Bethell, Donald; Schilling, Mark B.
Journal of Organic Chemistry, 1998 , vol. 63, # 8 p. 2774 - 2777
反应条件
in ethanol
T=0 - 20°C; Yield given;
参考文献
Page, Philip C. Bulman; Rassias, Gerasimos A.; Bethell, Donald; Schilling, Mark B.
Journal of Organic Chemistry, 1998 , vol. 63, # 8 p. 2774 - 2777
