三乙基(3-苯基丙氧基)硅烷合成路线 （共 33 条）
反应条件
triethylsilane; indium tribromide in chloroform
T=60°C; 1 h; Sealed tubeInert atmosphere; Mechanism; Reagent/catalyst;
参考文献
Moriya, Toshimitsu; Yoneda, Shinichiro; Kawana, Keita; Ikeda, Reiko; Konakahara, Takeo; Sakai, Norio
Journal of Organic Chemistry, 2013 , vol. 78, # 21 p. 10642 - 10650
参考文献
Glushkova,N.E.; Kharitonov,N.P.
J. Gen. Chem. USSR (Engl. Transl.), 1975 , vol. 45, p. 2018 - 2023,1981 - 1985
反应条件
hydrogen; palladium on activated charcoal in acetonitrile
T=20°C; 24 h; atmospheric pressure; Product distribution; Further Variations:Solvents;
参考文献
Ikawa, Takashi; Hattori, Kazuyuki; Sajiki, Hironao; Hirota, Kosaku
Tetrahedron, 2004 , vol. 60, # 32 p. 6901 - 6911
反应条件
2: 83 percent / Sc(OTf)3 / various solvent(s) / 1 h / 20 °C
View Scheme
参考文献
Suzuki; Watahiki; Oriyama
Tetrahedron Letters, 2000 , vol. 41, # 46 p. 8903 - 8906
反应条件
1: DCC / CHCl3 / 3 h / 20 °C
2: 97.2 percent / SmI2 / tetrahydrofuran; hexamethylphosphoric acid triamide / 0.08 h / 20 °C
View Scheme
参考文献
Honda, Toshio; Ishikawa, Fumihiro
Synthetic Communications, 1999 , vol. 29, # 19 p. 3323 - 3328
反应条件
1: indium tribromide / chloroform / 1 h / 20 °C / |Sealed tube; |Inert atmosphere
2: indium tribromide; triethylsilane / chloroform / 1 h / 60 °C / |Sealed tube; |Inert atmosphere
View Scheme
参考文献
Moriya, Toshimitsu; Yoneda, Shinichiro; Kawana, Keita; Ikeda, Reiko; Konakahara, Takeo; Sakai, Norio
Journal of Organic Chemistry, 2013 , vol. 78, # 21 p. 10642 - 10650
反应条件
indium tribromide in chloroform
T=20°C; 20 h; Mechanism;
参考文献
Sakai, Norio; Usui, Yuta; Ikeda, Reiko; Konakahara, Takeo
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 18 p. 3397 - 3401
反应条件
trimethylsilyl trifluoromethanesulfonate; boron trifluoride diethyl etherate in toluene
Product distribution; Further Variations:ReagentsSolvents;
参考文献
Morra, Nicholas A.; Pagenkopf, Brian L.
Synthesis, 2008 , # 4 p. 511 - 514
反应条件
dihydrogen hexachloroplatinate
参考文献
Lukevits,E.A.; Voronkov,M.G.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1965 , vol. 1, p. 116 - 121
Khimiya Geterotsiklicheskikh Soedinenii, 1965 , vol. 1, # 2 p. 179 - 186
反应条件
(i) Na, benzene, (ii) /BRN= 1732860/; Multistep reaction;
参考文献
Diekman,J. et al.
Journal of Organic Chemistry, 1967 , vol. 32, p. 3904 - 3919
