三乙基(3-苯基丙氧基)硅烷合成路线 （共 33 条）
反应条件
[Au(PPh3)]Cl; silver trifluoromethanesulfonate in 1,2-dichloro-ethane
T=20°C; 16 h;
参考文献
Shibata, Takanori; Kanda, Kazumasa; Ueno, Yasunori; Fujiwara, Ryo
Bulletin of the Chemical Society of Japan, 2006 , vol. 79, # 7 p. 1146 - 1147
反应条件
dirhodium(II) tetrakis(perfluorobutyrate) in dichloromethane
15 h; Ambient temperature;
参考文献
Doyle, Michael P.; High, Kenneth G.; Bagheri, Vahid; Pieters, Roland J.; Lewis, Patricia J.; Pearson, Matthew M.
Journal of Organic Chemistry, 1990 , vol. 55, # 25 p. 6082 - 6086
反应条件
[Rh(C5Me5)(1-(PMe(2,6-Me2C6H3))-2,6-Me2C6H3-κ-C6,P)][BArF] in dichloromethane-d2
T=25°C; 1 h; Inert atmosphereGlove box;
参考文献
Rubio, Miguel; Campos, Jesuus; Carmona, Ernesto
Organic Letters, 2011 , vol. 13, # 19 p. 5236 - 5239
反应条件
tris(pentafluorophenyl)-borane in benzene-d6
T=23°C; 0.5 h; GloveboxSchlenk technique;
参考文献
Bezier, David; Park, Sehoon; Brookhart, Maurice
Organic Letters, 2013 , vol. 15, # 3 p. 496 - 499
反应条件
hydrogen; palladium on activated charcoal in ethyl acetate
T=20°C; 24 h; Product distribution; Further Variations:Solvents;
参考文献
Sajiki, Hironao; Ikawa, Takashi; Hattori, Kazuyuki; Hirota, Kosaku
Chemical Communications, 2003 , # 5 p. 654 - 655
反应条件
1: 91 percent / Pd/C / toluene / 12 h / 110 °C
2: 99 percent / TBAF / dimethylformamide / 0.08 h / 20 °C
View Scheme
参考文献
Iida, Akira; Horii, Atsushi; Misaki, Tomonori; Tanabe, Yoo
Synthesis, 2005 , # 16 art. no. F06305SS, p. 2677 - 2682
反应条件
trimethylsilyl trifluoromethanesulfonate; boron trifluoride diethyl etherate in toluene
72 h;
参考文献
Morra, Nicholas A.; Pagenkopf, Brian L.
Synthesis, 2008 , # 4 p. 511 - 514
反应条件
trimethylsilyl trifluoromethanesulfonate; boron trifluoride diethyl etherate in toluene
72 h;
参考文献
Morra, Nicholas A.; Pagenkopf, Brian L.
Synthesis, 2008 , # 4 p. 511 - 514
反应条件
trimethylsilyl trifluoromethanesulfonate; boron trifluoride diethyl etherate in toluene
24 h;
参考文献
Morra, Nicholas A.; Pagenkopf, Brian L.
Synthesis, 2008 , # 4 p. 511 - 514
反应条件
trimethylsilyl trifluoromethanesulfonate; boron trifluoride diethyl etherate in toluene
120 h;
参考文献
Morra, Nicholas A.; Pagenkopf, Brian L.
Synthesis, 2008 , # 4 p. 511 - 514
