三乙基(3-苯基丙氧基)硅烷合成路线 （共 33 条）
反应条件
indium tribromide; trimethylsilyl iodide in chloroform T=60°C; 5 h; Sealed tubeInert atmosphere; Mechanism; Reagent/catalyst;
参考文献
Moriya, Toshimitsu; Yoneda, Shinichiro; Kawana, Keita; Ikeda, Reiko; Konakahara, Takeo; Sakai, Norio
Journal of Organic Chemistry, 2013 , vol. 78, # 21 p. 10642 - 10650
反应条件
1: indium tribromide; trimethylsilyl iodide / chloroform / 5 h / 60 °C / |Sealed tube; |Inert atmosphere 2: tetrabutyl ammonium fluoride / 5 h / 20 - 60 °C View Scheme
参考文献
Moriya, Toshimitsu; Yoneda, Shinichiro; Kawana, Keita; Ikeda, Reiko; Konakahara, Takeo; Sakai, Norio
Journal of Organic Chemistry, 2013 , vol. 78, # 21 p. 10642 - 10650
反应条件
water; scandium tris(trifluoromethanesulfonate) in acetonitrile 1 h; Ambient temperature;
参考文献
Oriyama, Takeshi; Kobayashi, Yoshinobu; Noda, Kojiro
Synlett, 1998 , # 10 p. 1047 - 1048
反应条件
1: indium tribromide; trimethylsilyl iodide / chloroform / 5 h / 60 °C / |Sealed tube; |Inert atmosphere 2: tetrabutyl-ammonium chloride / 5 h / 20 - 60 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 78, # 21 p. 10642 - 10650
反应条件
indium tribromide in toluene
2 h; Inert atmosphereReflux;
参考文献
Sridhar, Madabhushi; Raveendra, Jillella; China Ramanaiah, Beeram; Narsaiah, Chinthala
Tetrahedron Letters, 2011 , vol. 52, # 45 p. 5980 - 5982
反应条件
C48H48N2O4Ru2 in tetrahydrofuran
T=20°C; 24 h; IrradiationInert atmosphere; chemoselective reaction;
参考文献
Do, Youngshil; Han, Junghoon; Rhee, Young Ho; Park, Jaiwook
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 18 p. 3363 - 3366
反应条件
pyridinium p-toluenesulfonate; diethylazodicarboxylate in dichloromethane
T=20°C; 0.0833333 h;
参考文献
Hayashi, Minoru; Matsuura, Yutaka; Watanabe, Yutaka
Tetrahedron Letters, 2004 , vol. 45, # 7 p. 1409 - 1411
反应条件
tetrabutyl ammonium fluoride in N,N-dimethyl-formamide
T=20°C; 0.0833333 h;
参考文献
Iida, Akira; Horii, Atsushi; Misaki, Tomonori; Tanabe, Yoo
Synthesis, 2005 , # 16 art. no. F06305SS, p. 2677 - 2682
反应条件
samarium diiodide in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide
T=20°C; Etherification; 0.0833333 h;
参考文献
Honda, Toshio; Ishikawa, Fumihiro
Synthetic Communications, 1999 , vol. 29, # 19 p. 3323 - 3328
反应条件
scandium tris(trifluoromethanesulfonate) in various solvent(s)
T=20°C; 1 h;
参考文献
Suzuki; Watahiki; Oriyama
Tetrahedron Letters, 2000 , vol. 41, # 46 p. 8903 - 8906
