6H-苯并[c]苯并吡喃合成路线 (共 63 条)
反应条件
palladium diacetate; potassium carbonate; 2-Ph2P-2'-(Me2N)biphenyl in N,N-dimethyl acetamide
T=125°C; 2 h;
参考文献
Campeau, Louis-Charles; Parisien, Mathieu; Leblanc, Melissa; Fagnou, Keith
Journal of the American Chemical Society, 2004 , vol. 126, # 30 p. 9186 - 9187
反应条件
potassium carbonate; 1,3-bis(2,6-diisopropylphenyl)imidazolinium chloride; palladium in N,N-dimethyl acetamide
T=130°C; 24 h;
参考文献
Campeau, Louis-Charles; Thansandote, Praew; Fagnou, Keith
Organic Letters, 2005 , vol. 7, # 9 p. 1857 - 1860
反应条件
potassium acetate; palladium dihydroxide in N,N-dimethyl acetamide
T=145°C;
参考文献
Parisien, Mathieu; Valette, Damien; Fagnou, Keith
Journal of Organic Chemistry, 2005 , vol. 70, # 19 p. 7578 - 7584
反应条件
palladium diacetate; potassium carbonate; PCy3∙HBF4; silver carbonate in N,N-dimethyl acetamide
T=130°C;
参考文献
Campeau, Louis-Charles; Parisien, Mathieu; Jean, Annie; Fagnou, Keith
Journal of the American Chemical Society, 2006 , vol. 128, # 2 p. 581 - 590
反应条件
pyridine; 1,10-phenanthroline; potassium tert-butylate
T=20 - 160°C; 0.183333 h; Inert atmosphereMicrowave irradiation; regioselective reaction;
参考文献
Roman, Daniela Sustac; Takahashi, Yoko; Charette, Andre B.
Organic Letters, 2011 , vol. 13, # 12 p. 3242 - 3245
反应条件
tetrabutyl-ammonium chloride; palladium diacetate; caesium carbonate; triphenylphosphine in N,N-dimethyl-formamide
T=85 - 90°C; 2 h; Inert atmosphere;
参考文献
Jana, Rathin; Chatterjee, Indranil; Samanta, Shubhankar; Ray, Jayanta K.
Organic Letters, 2008 , vol. 10, # 21 p. 4795 - 4797
反应条件
pyridine; potassium tert-butylate
T=20 - 160°C; 0.183333 h; Inert atmosphereMicrowave irradiation; regioselective reaction;
参考文献
Roman, Daniela Sustac; Takahashi, Yoko; Charette, Andre B.
Organic Letters, 2011 , vol. 13, # 12 p. 3242 - 3245
反应条件
1: With n-butyl-magnesium bromide; n-butyllithium in tetrahydrofuran; hexane
T=0°C; Metallation; 0.5 h;
2: With titanium tetrachloride in tetrahydrofuran; hexane
T=0°C; Oxidation; self-coupling; 0.5 h;
参考文献
Inoue, Atsushi; Kitagawa, Kazuya; Shinokubo, Hiroshi; Oshima, Koichiro
Tetrahedron, 2000 , vol. 56, # 49 p. 9601 - 9605
反应条件
pyridine; potassium hexamethylsilazane
T=80°C; 16 h; Inert atmosphere;
参考文献
Roman, Daniela Sustac; Takahashi, Yoko; Charette, Andre B.
Organic Letters, 2011 , vol. 13, # 12 p. 3242 - 3245
反应条件
potassium peroxodisulfate; sodium hydroxide in water
T=100°C; 0.75 h;
参考文献
Pinter, Aron; Klussmann, Martin
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 4 p. 701 - 711