3-(环己基氨基)丙酸甲酯合成路线 （共 8 条）
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=0°C; Reflux;
参考文献
Banning, Joseph E.; Prosser, Anthony R.; Alnasleh, Bassam K.; Smarker, Jason; Rubina, Marina; Rubin, Michael
Journal of Organic Chemistry, 2011 , vol. 76, # 10 p. 3968 - 3986
反应条件
aluminum oxide
T=100 - 110°C; 1.5 h;
参考文献
Bosica, Giovanna; Spiteri, Jonathan; Borg, Caroline
Tetrahedron, 2014 , vol. 70, # 14 p. 2449 - 2454
反应条件
C12H18NO3S(1+)*HO4S(1-)
T=25°C; 0.416667 h; Ionic liquidNeat (no solvent); chemoselective reaction;
参考文献
Sun, Xudong; Du, Yijun; Li, Chunqing; Qi, Chenze
Kinetics and Catalysis, 2010 , vol. 51, # 5 p. 653 - 656
反应条件
[bmim]BF4; copper acetylacetonate
T=20°C; aza-Michael reaction; 0.25 h;
参考文献
Kantam, M. Lakshmi; Neeraja; Kavita; Neelima; Chaudhuri, Mihir K.; Hussain, Sahid
Advanced Synthesis and Catalysis, 2005 , vol. 347, # 6 p. 763 - 766
反应条件
1: HCl / 24 h / Ambient temperature
2: benzene / 14.5 h
View Scheme
参考文献
Atta-ur-Rahman; Ahmad, Viqar Uddin; Sultana, Mumtaz; Perveen, Nusrat; Sultana, Nighat
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1982 , vol. 37, # 6 p. 757 - 761
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in acetonitrile
T=25°C; Michael Addition; 2 h; Inert atmosphere;
参考文献
Peeters, Annelies; Ameloot, Rob; De Vos, Dirk E.
Green Chemistry, 2013 , vol. 15, # 6 p. 1550 - 1557
反应条件
in benzene
14.5 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Atta-ur-Rahman; Ahmad, Viqar Uddin; Sultana, Mumtaz; Perveen, Nusrat; Sultana, Nighat
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1982 , vol. 37, # 6 p. 757 - 761
反应条件
in benzene
14.5 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Atta-ur-Rahman; Ahmad, Viqar Uddin; Sultana, Mumtaz; Perveen, Nusrat; Sultana, Nighat
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1982 , vol. 37, # 6 p. 757 - 761
