4-[(4-硝基苯基)硫代]甲苯合成路线 (共 45 条)
反应条件
1: tin (II)-chloride; aq.-ethanolic hydrochloric acid / Hydrogenation 2: Diazotization View Scheme
参考文献
Law; Johnson
Journal of the American Chemical Society, 1930 , vol. 52, p. 3623,3625
反应条件
dihydrogen peroxide in acetic acid T=80°C; 3 h;
参考文献
Efremov, Yu. A.; Popova, A. G.; Khmel'nitskii, R. A.; Kaminskii, A. Ya; Fedyainov, N. V.
Journal of Organic Chemistry USSR (English Translation), 1980 , p. 944 - 949
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 5 p. 1072 - 1077
反应条件
1: hydrogen peroxide / acetic acid 2: S8, liq. NH3 / 6 h / 20 °C / other 4-nitrophenyl substituted phenyl sulfoxides, other arenesulfonamides View Scheme
参考文献
Chemistry Letters, , p. 535 - 538
反应条件
sulfur in ammonia T=100°C; 4 h; variation of temperature; Product distributionMechanism;
参考文献
Phosphorus and Sulfur and the Related Elements, , vol. 19, p. 205 - 212
反应条件
1: aqueous H2O2; glacial acetic acid / auf Siedetemperatur 2: bromine / 190 °C View Scheme
参考文献
Elliott; Harington
Journal of the Chemical Society, 1949 , p. 1374,1376
反应条件
sulfur in ammonia T=100°C; 4 h; variation of temperature; Product distributionMechanism;
参考文献
Phosphorus and Sulfur and the Related Elements, , vol. 19, p. 205 - 212
反应条件
1: hydrogen peroxide / acetic acid 2: S8, liq. NH3 / 6 h / 20 °C / other 4-nitrophenyl substituted phenyl sulfoxides, other arenesulfonamides View Scheme
参考文献
Sato, Ryu; Chiba, Shuji; Takikawa, Yuji; Takizawa, Saburo; Saito, Minoru
Chemistry Letters, 1983 , p. 535 - 538
反应条件
sulfur in ammonia T=100°C; 4 h; variation of temperature; Product distributionMechanism;
参考文献
Sato, Ryu; Chiba, Shuji; Saito, Nobushige; Sato, Mikiya; Saito, Minoru
Phosphorus and Sulfur and the Related Elements, 1984 , vol. 19, p. 205 - 212
反应条件
hydrogen; Raney Ni (W2) in methanol T=45°C; P=3000.2 Torr; 6 h;
参考文献
Kansy, M; Seydel, JK; Wiese, M; Haller, R
European Journal of Medicinal Chemistry, 1992 , vol. 27, # 3 p. 237 - 244
反应条件
caesium carbonate in N,N-dimethyl-formamide
T=110°C; Ullmann reaction; 5 h; Inert atmosphere;
参考文献
Prasad; Naidu, Ajay B.; Sekar
Tetrahedron Letters, 2009 , vol. 50, # 13 p. 1411 - 1415