二(2,3,4,5,6-五氟苯基)二氮烯合成路线 (共 3 条)
反应条件
lithium aluminium tetrahydride in diethyl ether refluxing (0.5 h);
参考文献
Gmelin Handbook: F: PerFHalOrg.8, 3, page 55 - 151
反应条件
potassium hydroxide in tert-butyl alcohol 2 h; Heating;
参考文献
Jarman; Barrie; Deadman; Houghton; McCague; Rowlands
Journal of Medicinal Chemistry, 1990 , vol. 33, # 9 p. 2452 - 2455
反应条件
2: NaOMe / methanol
3: aq. H2O2, (CF3CO)2O
View Scheme
参考文献
Burdon,J. et al.
Journal of the Chemical Society, 1965 , p. 2621 - 2627