3-甲基-2-丁烯酸叔丁酯合成路线 （共 7 条）
反应条件
n-butyllithium; diisopropylamine in tetrahydrofuran; hexane T=-30 - 25°C; 1.5 h; Irradiation;
参考文献
Russell, Glen A.; Mudryk, Boguslaw; Ros, Francisco; Jawdosiuk, Mikolaj
Tetrahedron, 1982 , vol. 38, # 8 p. 1059 - 1068
反应条件
potassium tert-butylate; 18-crown-6 ether in diethyl ether 2 h; Ambient temperature;
参考文献
Mayr, Herbert; Brueggen, Uwe von der
Chemische Berichte, 1988 , vol. 121, p. 339 - 346
反应条件
pyridine; thionyl chloride; benzene
参考文献
Hauser; Puterbaugh
Journal of the American Chemical Society, 1953 , vol. 75, p. 1068,1069, 1071
反应条件
1: diethyl ether; lithium amide; ammonia / beim Erwaermen des Reaktionsgemisches mit Aceton 2: thionyl chloride; benzene; pyridine View Scheme
参考文献
Hauser; Puterbaugh
Journal of the American Chemical Society, 1953 , vol. 75, p. 1068,1069, 1071
反应条件
sulfuric acid in dichloromethane
参考文献
Johnson,P.Y.; Berchtold,G.A.
Journal of Organic Chemistry, 1970 , vol. 35, p. 584 - 592
反应条件
(i) LDA, THF, hexane, (ii) /BRN= 635680/; Multistep reaction;
参考文献
Hartzell,S.L. et al.
Tetrahedron Letters, 1974 , p. 1403 - 1406
反应条件
in benzene T=30°C; Acylation; alcoholysis; KineticsActivation energy; Further Variations:Temperatures;
参考文献
Marshalok; Oglashennyi; Makitra; Pirig; Yatchishin
Russian Journal of Organic Chemistry, 1998 , vol. 34, # 10 p. 1410 - 1418
