4-苯甲基-1,3-苯二酚合成路线 （共 17 条）
反应条件
1: With boron tribromide in dichloromethane T=-15 - 20°C; 18 h; 2: With water in dichloromethane T=20°C;
参考文献
Petronzi, Carmen; Filosa, Rosanna; Peduto, Antonella; Monti, Maria Chiara; Margarucci, Luigi; Massa, Antonio; Ercolino, Simona Francesca; Bizzarro, Valentina; Parente, Luca; Riccio, Raffaele; De Caprariis, Paolo
European Journal of Medicinal Chemistry, 2011 , vol. 46, # 2 p. 488 - 496
反应条件
1: With sodium tetrahydroborate in tetrahydrofuran; water T=0 - 20°C; 61 h; 2: With sodium hydroxide in water 1 h; Heating / reflux; 3: With hydrogenchloride in water
参考文献
WO2004/72051 A1, ;
Page 38; 39 ;
反应条件
ethanol; sodium ethanolate anschliessendes Behandeln mit wss. HCl;
参考文献
Justus Liebigs Annalen der Chemie, , vol. 612, p. 78,88
Bulletin de la Societe Chimique de France, , vol. <5> 2, p. 1737,1740
反应条件
1: With antimony trichloride in acetonitrile T=65°C; 0.416667 h; Microwave irradiation; 2: With boron tribromide in dichloromethane T=-20 - 0°C;
参考文献
Synlett, , # 11 p. 1585 - 1591
反应条件
hydrogenchloride; amalgamated zinc
参考文献
Journal of the American Chemical Society, , vol. 48, p. 793
反应条件
trifluoroacetic acid in chloroform 96 h; RefluxInert atmosphere;
参考文献
Synthesis, , # 24 art. no. M03209SS, p. 4190 - 4202
反应条件
CoCl2 T=140°C; 0.5 h;
参考文献
Chemistry Letters, , p. 173 - 176
反应条件
1: Darstellung durch Kondensation und nachfolgende Hydrolyse nach Hoesch 2: amalgamated zinc; hydrochloric acid View Scheme
参考文献
Journal of the American Chemical Society, , vol. 48, p. 793
反应条件
1: Darstellung durch Kondensation und nachfolgende Hydrolyse nach Hoesch 2: amalgamated zinc; hydrochloric acid View Scheme
参考文献
Journal of the American Chemical Society, , vol. 48, p. 793
反应条件
1.1: potassium phosphate; palladium diacetate; triphenylphosphine / toluene / 16 h / 100 °C / Inert atmosphere 2.1: boron tribromide / dichloromethane / 18 h / -15 - 20 °C 2.2: 20 °C View Scheme
参考文献
European Journal of Medicinal Chemistry, , vol. 46, # 2 p. 488 - 496
