4-甲氧基苯基 异硫氰酸酯合成路线 (共 89 条)
反应条件
1: With triethylamine in ethanol T=20°C; 2: With 4-(N,N-dimethlyamino)pyridine; di-tert-butyl dicarbonate in ethanol T=20°C; 0.25 h; Further stages.;
参考文献
Munch, Henrik; Hansen, Jon S.; Pittelkow, Michael; Christensen, Jorn B.; Boas, Ulrik
Tetrahedron Letters, 2008 , vol. 49, # 19 p. 3117 - 3119
反应条件
triethylamine; thiourea in tetrahydrofuran Ambient temperature;
参考文献
Kim, Jae Nyoung; Ryu, Eung K.
Tetrahedron Letters, 1993 , vol. 34, # 51 p. 8283 - 8284
反应条件
sodium hydrogencarbonate in dichloromethane; water T=0 - 20°C; 1 h;
参考文献
Wroblewska, Aneta; Mloston, Grzegorz
Phosphorus, Sulfur and Silicon and the Related Elements, 2013 , vol. 188, # 4 p. 509 - 511
反应条件
iodine; triethylamine in acetonitrile T=5°C; Cooling with ice;
参考文献
Nath, Jayashree; Ghosh, Harisadhan; Yella, Mamesh; Patel, Bhisma K.
European Journal of Organic Chemistry, 2009 , # 12 p. 1849 - 1851
反应条件
ethylmagnesium bromide in tetrahydrofuran T=50°C; 0.5 h;
参考文献
Besson, Thierry; Guillard, Jerome; Rees, Charles W.; Thiery, Valerie
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 5 p. 889 - 892
反应条件
sulfur; [Rh(H)(PEt3)3] in acetone 6 h; Heating;
参考文献
Arisawa, Mieko; Ashikawa, Masanori; Suwa, Atsushi; Yamaguchi, Masahiko
Tetrahedron Letters, 2005 , vol. 46, # 10 p. 1727 - 1729
反应条件
sodium hydroxide in dichloromethane T=20°C; 1 h;
参考文献
Li, Zheng-Yi; Ma, Hong-Zhao; Han, Chen; Xi, Hai-Tao; Meng, Qi; Chen, Xin; Sun, Xiao-Qiang
Synthesis (Germany), 2013 , vol. 45, # 12 art. no. SS-2013-F0228-OP, p. 1667 - 1674
反应条件
bis(trichloromethyl) carbonate; sulfur; triethylamine; selenium in dichloromethane 6.5 h; Heating;
参考文献
Shan; Bian; Su; Liang
Organic Preparations and Procedures International, 2004 , vol. 36, # 3 p. 283 - 286
反应条件
[bis(acetoxy)iodo]benzene; triethylamine
参考文献
Ghosh, Harisadhan; Yella, Ramesh; Nath, Jayashree; Patel, Bhisma K.
European Journal of Organic Chemistry, 2008 , # 36 p. 6189 - 6196
反应条件
sodium hydroxide; potassium carbonate in acetonitrile T=25°C; 1.5 h;
参考文献
Albanese; Penso
Synthesis, 1991 , # 11 p. 1001 - 1002