2-乙烯基-N,N-二甲基苄胺合成路线 （共 14 条）
反应条件
sodium hydroxide; Et3N-BH3; dihydrogen peroxide other hydroboration agent; Product distribution;
参考文献
Kafka, Stanislav; Trska, Petr; Kytner, Jan; Taufmann, Petr; Ferles, Miloslav
Collection of Czechoslovak Chemical Communications, 1987 , vol. 52, # 8 p. 2047 - 2056
参考文献
Bersch; Meyer
Archiv der Pharmazie (Weinheim, Germany), 1954 , vol. 287, p. 613,616
参考文献
v. Braun
Chemische Berichte, 1917 , vol. 50, p. 47
反应条件
in methanol
T=20°C; Substitution; P=1125.09 Torr; 1.5 h;
参考文献
Ritleng, Vincent; Sutter, Jean Pascal; Pfeffer, Michel; Sirlin, Claude
Chemical Communications, 2000 , # 2 p. 129 - 130
反应条件
tetrabutyl ammonium fluoride; acrylic acid methyl ester in acetonitrile
2 h; Ambient temperature; Yield given;
参考文献
Ito; Nakatsuka; Saegusa
Journal of the American Chemical Society, 1982 , vol. 104, # 26 p. 7609 - 7622
反应条件
cesium fluoride in N,N-dimethyl-formamide
3 h; Ambient temperature;
参考文献
Sato, Yoshiro; Shirai, Naohiro; Machida, Yoshio; Ito, Emiko; Yasui, Takayo; et al.
Journal of Organic Chemistry, 1992 , vol. 57, # 25 p. 6711 - 6716
反应条件
1: 1.) n-BuLu, 2.) Et3N / 1.) THF, -50 deg C -> -40 deg C, 1 h, 2.) -50 deg C -> -40 deg C. 0.5 h; room temperature, 2 h
3: methyl acrylate, n-Bu4NF / acetonitrile / 2 h / Ambient temperature
View Scheme
参考文献
Ito; Nakatsuka; Saegusa
Journal of the American Chemical Society, 1982 , vol. 104, # 26 p. 7609 - 7622
反应条件
2: methyl acrylate, n-Bu4NF / acetonitrile / 2 h / Ambient temperature
View Scheme
参考文献
Ito; Nakatsuka; Saegusa
Journal of the American Chemical Society, 1982 , vol. 104, # 26 p. 7609 - 7622
反应条件
silver(l) oxide in water
1 h;
参考文献
Kafka, Stanislav; Trska, Petr; Kytner, Jan; Taufmann, Petr; Ferles, Miloslav
Collection of Czechoslovak Chemical Communications, 1987 , vol. 52, # 8 p. 2047 - 2056
反应条件
sodium amalgam; water
参考文献
Emde
Justus Liebigs Annalen der Chemie, 1912 , vol. 391, p. 93
Chem. Zentralbl., 1910 , vol. 81, # II p. 1478
