2,4,6-三甲基苯甲酸甲酯合成路线 （共 50 条）
反应条件
sulfuric acid T=148 - 159°C; P=9375.7 Torr; 0.0866667 h; Irradiation;
参考文献
Cablewski, Teresa; Faux, Alan F.; Strauss, Christopher R.
Journal of Organic Chemistry, 1994 , vol. 59, # 12 p. 3408 - 3412
反应条件
in methanol; benzene 0.5 h; Ambient temperature;
参考文献
Mashimoto, Norio; Aoyama, Toyohiko; Shioiri, Takayuki
Chemical & Pharmaceutical Bulletin, 1981 , vol. 29, # 5 p. 1475 - 1478
反应条件
1: (2,4,6-trimethylphenyl)methyl alcohol With sodium chlorite; sodium dihydrogenphosphate; 1-MeAZADO(1+)*Cl(1-) in dichloromethane; water T=25°C; 4.5 h; 2: With 2-methyl-but-2-ene in dichloromethane; water 3: diazomethane With hydrogenchloride; sodium hydroxide Product distribution / selectivity; more than 3 stages;
参考文献
Nissan Chemical Industries, Ltd.
Patent: US2009/124806 A1, 2009 ;
Location in patent: Page/Page column 5-6 ;
反应条件
N-bromosuccinmide in toluene T=100°C; 1 h;
参考文献
Zhang, Ningning; Yang, Rui; Zhang-Negrerie, Daisy; Du, Yunfei; Zhao, Kang
Journal of Organic Chemistry, 2013 , vol. 78, # 17 p. 8705 - 8711
参考文献
Shibuya, Masatoshi; Sato, Takahisa; Tomizawa, Masaki; Iwabuchi, Yoshiharu
Chemical Communications, 2009 , # 13 p. 1739 - 1741
反应条件
copper(ll) bromide in acetonitrile 0.1 h; Ambient temperature;
参考文献
Kim, Sunggak; Lee, Jae In
Journal of Organic Chemistry, 1984 , vol. 49, # 10 p. 1712 - 1716
反应条件
potassium hydroxide; Aliquatreg; 336 T=20°C; 1 h;
参考文献
Loupy, Andre; Pedoussaut, Michel; Sansoulet, Jean
Journal of Organic Chemistry, 1986 , vol. 51, # 5 p. 740 - 742
反应条件
lithium hydroxide in tetrahydrofuran Methylation; esterification; 3 h; Heating;
参考文献
Chakraborti, Asit K.; Basak, Anindita; Grover, Vikas
Journal of Organic Chemistry, 1999 , vol. 64, # 21 p. 8014 - 8017
反应条件
potassium carbonate in acetonitrile 4 h; Heating;
参考文献
Yoshino, Tomonori; Togo, Hideo
Synlett, 2005 , # 3 art. no. U29304ST, p. 517 - 519
反应条件
tris(triphenylphosphine)-palladium(II) dichloride T=75°C; P=5171.5 Torr; 5 h;
参考文献
Baird, William C.; Hartgerink, Ronald L.; Surridge, John H.
Journal of Organic Chemistry, 1985 , vol. 50, # 23 p. 4601 - 4605
