10-氯-9,10-二氢-9-氧杂-10-磷杂菲合成路线 （共 10 条）
反应条件
zinc(II) chloride; phosphorus trichoride T=20 - 180°C; 7 h;
参考文献
Su, Wen-Chiung; Lin, Chang-Chih; Sheng, Ching-Shang
Patent: US2007/173659 A1, 2007 ;
Location in patent: Page/Page column 4 ;
反应条件
zinc(II) chloride T=150°C; 2 h;
参考文献
Abranyi-Balogh, Peter; Keglevich, Gyoergy
Synthetic Communications, 2011 , vol. 41, # 10 p. 1421 - 1426
反应条件
Zinc chloride in toluene
反应条件
phosphorus trichoride in chloroform 3 h; Inert atmosphereReflux;
参考文献
Synthetic Communications, , vol. 41, # 10 p. 1421 - 1426
反应条件
water; hydrogenchloride T=80°C; 1 h; Product distribution / selectivity;
参考文献
UFC CORPORATION
Patent: US2011/34717 A1, 2011 ;
Location in patent: Page/Page column 3 ;
参考文献
Toyo Boseki Kabushiki Kaisha
Patent: US6245880 B1, 2001 ;
反应条件
in tetrahydrofuran; water; ethyl acetate
参考文献
Meng, Xiangtai; Huang, You; Chen, Ruyu
Chemistry - A European Journal, 2008 , vol. 14, # 23 p. 6852 - 6856
反应条件
in tetrahydrofuran T=26°C; 20 h;
参考文献
Keglevich, Gyoergy; Kerenyi, Andrea; Szelke, Helga; Ludanyi, Krisztina; Koertvelyesi, Tamas
Journal of Organometallic Chemistry, 2006 , vol. 691, # 23 p. 5038 - 5044
反应条件
in tetrahydrofuran; diethyl ether T=26°C; 20 h;
参考文献
Keglevich, Gyoergy; Szelke, Helga; Kerenyi, Andrea; Imre, Timea; Ludanyi, Krisztina; Dukai, Jozsef; Nagy, Ferenc; Aranyi, Peter
Heteroatom Chemistry, 2004 , vol. 15, # 6 p. 459 - 463
反应条件
1: bromobenzene With iodine; magnesium T=50°C; 2 h; Inert atmosphereReflux; 2: 6-chloro-(6H)dibenzo[c,e][1,2]oxaphosphorin T=25°C; Inert atmosphereReflux; 3: With water; ammonium chloride T=0°C; Inert atmosphere;
参考文献
Liu, Yuanyuan; Yang, Guoqiang; Yao, Dongmei; Tian, Fengtao; Zhang, Wanbin
Science China Chemistry, 2011 , vol. 54, # 1 p. 87 - 94
