4,4-二甲基-2-环戊烯-1-酮合成路线 (共 40 条)
反应条件
boron trifluoride diethyl etherate in dichloromethane T=0°C; 2 h;
参考文献
Journal of the American Chemical Society, , vol. 103, p. 1996
反应条件
potassium hydroxide in tetrahydrofuran; diethyl ether 48 h; Heating;
参考文献
Magnus, P. D.; Nobbs, M. S.
Synthetic Communications, 1980 , vol. 10, # 4 p. 273 - 278
参考文献
Salomon; Coughlin; Ghosh; Zagorski
Journal of the American Chemical Society, 1982 , vol. 104, # 4 p. 998 - 1007
反应条件
phosphoric acid Heating;
参考文献
Holder, Richard W.; Daub, John P.; Baker, Wesley E.; Gilbert, Raymond H; Graf, Norman A.
Journal of Organic Chemistry, 1982 , vol. 47, # 8 p. 1445 - 1451
反应条件
1: PdCl2; CuCl; O2 / dimethylformamide; H2O / 72 h 2: KOH / tetrahydrofuran; diethyl ether / 96 h / Heating View Scheme
参考文献
Journal of the American Chemical Society, , vol. 125, # 6 p. 1567 - 1574
参考文献
Journal of the American Chemical Society, , vol. 93, p. 5513 - 5520
Journal of Organic Chemistry, , vol. 26, p. 3525 - 3527
反应条件
1: 98 percent / Dibal-H / pentane / 3 h / -78 - 20 °C 2: PdCl2; CuCl; O2 / dimethylformamide; H2O / 72 h 3: KOH / tetrahydrofuran; diethyl ether / 96 h / Heating View Scheme
参考文献
Journal of the American Chemical Society, , vol. 125, # 6 p. 1567 - 1574
反应条件
1: CF3SO3Cu / diethyl ether / Irradiation 2: CrO3, H2SO4 3: 600 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 101, # 14 p. 3961 - 3963
反应条件
1: 92 percent / H2SO4 / toluene 2: 79 percent / sodium / toluene / 28 h 3: 87 percent / 85 percent phosphoric acid / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 47, # 8 p. 1445 - 1451
反应条件
1: Na, liq. NH3 / diethyl ether 2: polyphosphoric acid View Scheme
参考文献
Journal of Organic Chemistry, , vol. 26, p. 3525 - 3527