5-氯-4-硝基-2,1,3-苯并噻二唑合成路线 （共 8 条）
反应条件
sulfuric acid; nitric acid
参考文献
Zhurnal Obshchei Khimii, , vol. 27, p. 2599,2603; engl. Ausg. S. 2656, 2659
反应条件
1: SOCl2, Py / 75 - 80 °C 2: NaNO3, H2SO4 / 95 - 100 °C View Scheme
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 3, p. 662 - 666
Khimiya Geterotsiklicheskikh Soedinenii, , vol. 3, # 5 p. 839 - 844
参考文献
Pesin; Chalezkii
Zhurnal Obshchei Khimii, 1957 , vol. 27, p. 2599,2603; engl. Ausg. S. 2656, 2659
反应条件
chlorine; iron T=150°C;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 2, p. 405 - 407
Khimiya Geterotsiklicheskikh Soedinenii, , vol. 2, # 4 p. 541 - 544
反应条件
1: aq. NaN3 / dimethylsulfoxide 2: P(OEt)3 / Heating View Scheme
参考文献
Ghosh,P.B.; Everitt,B.J.
Journal of Medicinal Chemistry, 1974 , vol. 17, # 2 p. 203 - 206
反应条件
ammonia in ethylene glycol T=180 - 200°C;
参考文献
Pesin,V.G. et al.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1968 , vol. 4, p. 186 - 188
Khimiya Geterotsiklicheskikh Soedinenii, 1968 , vol. 4, # 2 p. 249 - 253
反应条件
sodium azide; N-ethyl-N-methylpyrrolidinium tetrafluoroborate; tetrabutylammomium bromide in water T=80°C; 2 h;
参考文献
Sheremetev, Aleksei B.; Aleksandrova, Nataliya S.; Ignat'Ev, Nikolai V.; Schulte, Michael
Mendeleev Communications, 2012 , vol. 22, # 2 p. 95 - 97
反应条件
1: NH3 / ethane-1,2-diol / 180 - 200 °C
2: aq. NaHS / Heating
View Scheme
参考文献
Pesin,V.G. et al.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1968 , vol. 4, p. 186 - 188
Khimiya Geterotsiklicheskikh Soedinenii, 1968 , vol. 4, # 2 p. 249 - 253
