3,4-二氢-4-甲基-2H-吡喃合成路线 （共 10 条）
反应条件
ruthenium(IV) oxide; sodium periodate in tetrachloromethane 50 h;
参考文献
Torii, Sigeru; Inokuchi, Tsutomu; Kondo, Kazumi
Journal of Organic Chemistry, 1985 , vol. 50, # 24 p. 4980 - 4982
反应条件
Cl2Ni(1,2-bis(diphenylphosphino)ethane) in tetrahydrofuran
T=80°C; 4 h;
参考文献
Guagnano, Vito; Lardicci, Luciano; Malanga, Corrado; Menicagli, Rita
Tetrahedron Letters, 1998 , vol. 39, # 14 p. 2025 - 2026
反应条件
phosphorus pentoxide
参考文献
Parham; Holmquist
Journal of the American Chemical Society, 1951 , vol. 73, p. 913
反应条件
niobium phosphate
T=299.84°C; 3.33333 h; Temperature;
参考文献
Sushkevich; Ordomsky; Ivanova
Applied Catalysis A: General, 2012 , vol. 441-442, p. 21 - 29
反应条件
aluminum oxide; sodium in n-heptane
T=60°C; 2 h; other time, temperature; Product distribution;
参考文献
Ibatullin, U. G.; Petrushina, T. F.; Akhmadeeva, A. A.; Safarov, M. G.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1985 , vol. 21, # 3 p. 262 - 264
Khimiya Geterotsiklicheskikh Soedinenii, 1985 , vol. 21, # 3 p. 318 - 320
反应条件
1: KHMDS / tetrahydrofuran; toluene / 0.17 h / -78 °C
2: (Bu3Sn)(Bu)CuLi*CN / tetrahydrofuran / -78 °C
View Scheme
参考文献
Wildman, Tanya; Kocienski, Philip J.; Narquizian, Robert; Whittingham, William G.
Synthesis, 2002 , # 3 p. 393 - 398
反应条件
1: 47 percent / NaBH4
2: KHMDS / tetrahydrofuran; toluene / 0.17 h / -78 °C
3: (Bu3Sn)(Bu)CuLi*CN / tetrahydrofuran / -78 °C
View Scheme
参考文献
Wildman, Tanya; Kocienski, Philip J.; Narquizian, Robert; Whittingham, William G.
Synthesis, 2002 , # 3 p. 393 - 398
反应条件
sodium hydroxide; pentacarbonyliron(0)
T=180°C; 10 h; autoclave, other time; Product distribution;
参考文献
Ibatullin, U. G.; Petrushina, T. F.; Akhmadeeva, A. A.; Safarov, M. G.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1985 , vol. 21, # 3 p. 262 - 264
Khimiya Geterotsiklicheskikh Soedinenii, 1985 , vol. 21, # 3 p. 318 - 320
反应条件
sodium hydroxide; pentacarbonyliron(0)
T=180°C; 10 h; autoclave, other time; Product distribution;
参考文献
Ibatullin, U. G.; Petrushina, T. F.; Akhmadeeva, A. A.; Safarov, M. G.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1985 , vol. 21, # 3 p. 262 - 264
Khimiya Geterotsiklicheskikh Soedinenii, 1985 , vol. 21, # 3 p. 318 - 320
反应条件
sodium hydroxide-kieselguhr-catalyst
参考文献
Union Carbide Corp.
Patent: US2858322 , 1956 ;
