addition of CF3 radicals (glow discharge of C2F6 below 50°C) to SnI4;; condensation at -196°C, extraction (benzene) and gaschromatographic separation;;
参考文献
Lagow et al.
Journal of the American Chemical Society, 1975 , vol. 97, p. 518
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Gmelin Handbook: F: PerFHalOrg.4, 4.3.1, page 181 - 183
in neat (no solvent)
Kinetics; byproducts: C2F6; reaction of CF3-radical on fused SiO2 in the presence of H2O on the surface; monitored by mass-spectroscopy;
参考文献
Selamoglu, N.; Rossi, M.J.; Golden, D.M.
Journal of Chemical Physics, 1986 , vol. 84, # 4 p. 2400 - 2407
