4-杂氮三环[4.3.1.13,8]十一烷-5-酮合成路线 （共 21 条）
反应条件
sodium hydroxide; benzenesulfonyl chloride 1.) below 30 deg C, 2.) 55 deg C, 2h;
参考文献
St. Georgiev; Saeva; Kinsolving
Journal of Heterocyclic Chemistry, 1986 , vol. 23, # 4 p. 1023 - 1025
反应条件
1: 4-chloro-4-azatricyclo[4.3.1.1(3,8)]undecan-5-one in dichloromethane T=-78°C; Photolysis; 2: methanol With triethylamine in dichloromethane T=20°C; 2 h;
参考文献
Tetrahedron Letters, , vol. 47, # 25 p. 4285 - 4288
反应条件
sodium azide; methanesulfonic acid in acetic acid 1 h; Ambient temperature;
参考文献
Tetrahedron, , vol. 41, # 18 p. 3753 - 3762
反应条件
sodium azide; methanesulfonic acid 1 h; Ambient temperature;
参考文献
Tetrahedron, , vol. 41, # 18 p. 3753 - 3762
反应条件
triethyl borane; oxygen in dichloromethane T=-78°C; UV-irradiationInert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 75, # 8 p. 2610 - 2618
反应条件
iron(II) sulfate in methanol 4 h; Ambient temperature;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 21, # 1 p. 97 - 103
Zhurnal Organicheskoi Khimii, , vol. 21, # 1 p. 107 - 113
反应条件
T=150 - 170°C; 0.0833333 h;
参考文献
Novoselov, E. F.; Isaev, S. D.; Yurchenko, A. G.; Vodichka, L.; Trshiska, Ya.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, # 12 p. 2284 - 2289
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 12 p. 2558 - 2564
反应条件
in toluene T=200°C; 1 h;
参考文献
Tetrahedron Letters, , vol. 47, # 25 p. 4285 - 4288
反应条件
in water 0.166667 h; Ambient temperature;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 17, # 12 p. 2284 - 2289
Zhurnal Organicheskoi Khimii, , vol. 17, # 12 p. 2558 - 2564
反应条件
1: 6 percent / NH3, monoperoxy-o-phthalic acid / methanol; diethyl ether / 0.33 h / 0 - 5 °C 2: 28 percent / FeSO4*7H2O / methanol / 4 h / Ambient temperature View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 21, # 1 p. 97 - 103
Zhurnal Organicheskoi Khimii, , vol. 21, # 1 p. 107 - 113
