1,2,5,6-二苯并吩嗪合成路线 (共 25 条)
反应条件
potassium tert-butylate; oxygen in toluene
参考文献
Piechowska, Joanna; Virkki, Kirsi; Sadowski, Bartlomiej; Lemmetyinen, Helge; Tkachenko, Nikolai V.; Gryko, Daniel T.
Journal of Physical Chemistry A, 2014 , vol. 118, # 1 p. 144 - 151
反应条件
KO2 in toluene
T=80°C; 8 h;
参考文献
Crank, George; Makin, Mohammad I. H.
Australian Journal of Chemistry, 1984 , vol. 37, # 4 p. 845 - 855
反应条件
water; calcium chloride
T=40 - 50°C;
参考文献
Raschig
Z. Ang., 1907 , vol. 20, p. 2070
Full Text Show Details
Claus; Jaeck
Patent: DE78748 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 4, p. 373
Full Text Show Details
Meigen; Normann
Chemische Berichte, 1900 , vol. 33, p. 2714,2715
参考文献
Mayer, Roland
Phosphorus and Sulfur and the Related Elements, 1985 , vol. 23, p. 277 - 296
反应条件
ethylmagnesium bromide in tetrahydrofuran
1.) 50-55 deg C, 3 h, 2.) r.t., overnight; Yield given;
参考文献
Kosugi, Yoshio; Itoho, Kazuo; Okazaki, Hiroshi; Yanai, Tomoko
Journal of Organic Chemistry, 1995 , vol. 60, p. 5690 - 5692
反应条件
hydrogenchloride in methanol
Irradiationalso in presence of 0.015M KCN/MeCN-H2O; Further byproducts given;
参考文献
Albini, Angelo; Bettinetti, Gian Franco; Fasani, Elisa; Pietra, Silvio
Gazzetta Chimica Italiana, 1982 , vol. 112, # 1/2 p. 13 - 18
反应条件
in various solvent(s)
T=155°C; 12 h;
参考文献
Nay, Barry; Scriven, Eric F. V.; Suschitzky, Hans; Thomas, Desmond R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 611 - 613
反应条件
in various solvent(s)
T=155°C; 12 h;
参考文献
Nay, Barry; Scriven, Eric F. V.; Suschitzky, Hans; Thomas, Desmond R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 611 - 613
反应条件
potassium superoxide in toluene
T=80°C; 8 h;
参考文献
Crank, G.; Makin, M. I. H.
Tetrahedron Letters, 1983 , vol. 24, # 30 p. 3159 - 3160
反应条件
potassium hydroxide
T=55°C;
参考文献
Meisenheimer; Witte
Chemische Berichte, 1903 , vol. 36, p. 4157,4163