反应条件
in hydrogen fluoride HF (liquid); absence of air and moisture; distn. of HF on K-salt, warming to -78°C, further warming to dissoln. of K-salt; pptn. on cooling (-78°C); further crop by solvent removal (vac., -78°C) and sublimation (vac.);
参考文献
Gillespie, Ronald J.; Spekkens, Paul H.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1977 , p. 1539 - 1546
