4-甲氧基呋喃并[2,3-b]喹啉-8-醇合成路线 (共 9 条)
反应条件
trifluoroacetic acid in chloroform
参考文献
Boyd, Derek R.; Sharma, Narain D.; Carroll, Jonathan G.; Loke, Pui L.; O'Dowd, Colin R.; Allen, Christopher C. R.
RSC Advances, 2013 , vol. 3, # 27 p. 10944 - 10955
反应条件
1: 90 percent / acetonitrile
2: 68 percent / NBS / CCl4
3: 90 percent / NaOMe
4: TFA
View Scheme
参考文献
Boyd, Derek R.; Sharma, Narain D.; O'Dowd, Colin R.; Carroll, Jonathan G.; Loke, Pui L.; Allen, Christopher C. R.
Chemical Communications, 2005 , # 31 p. 3989 - 3991
反应条件
1: Sphingomonas yanoikuyae B8/36 / |Microbiological reaction
2: trifluoroacetic acid / chloroform
View Scheme
参考文献
Boyd, Derek R.; Sharma, Narain D.; Carroll, Jonathan G.; Loke, Pui L.; O'Dowd, Colin R.; Allen, Christopher C. R.
RSC Advances, 2013 , vol. 3, # 27 p. 10944 - 10955
反应条件
1: sodium methylate / 2 h / |Reflux; |Inert atmosphere
2: Sphingomonas yanoikuyae B8/36 / |Microbiological reaction
3: trifluoroacetic acid / chloroform
View Scheme
参考文献
Boyd, Derek R.; Sharma, Narain D.; Carroll, Jonathan G.; Loke, Pui L.; O'Dowd, Colin R.; Allen, Christopher C. R.
RSC Advances, 2013 , vol. 3, # 27 p. 10944 - 10955
反应条件
1: diphenyl ether / 235 - 255 °C
2: NaBH4, aq. NaOH / methanol
3: POCl3 / 1 h / Heating
4: methanol / 3 h / Heating
5: aq. HCl / ethanol / 1 h / Heating
View Scheme
参考文献
Ramachandran,V.N. et al.
Indian Journal of Chemistry, 1973 , vol. 11, p. 1088 - 1091
反应条件
1: POCl3 / 1 h / Heating
2: methanol / 3 h / Heating
3: aq. HCl / ethanol / 1 h / Heating
View Scheme
参考文献
Ramachandran,V.N. et al.
Indian Journal of Chemistry, 1973 , vol. 11, p. 1088 - 1091
反应条件
1: NaBH4, aq. NaOH / methanol
2: POCl3 / 1 h / Heating
3: methanol / 3 h / Heating
4: aq. HCl / ethanol / 1 h / Heating
View Scheme
参考文献
Ramachandran,V.N. et al.
Indian Journal of Chemistry, 1973 , vol. 11, p. 1088 - 1091
反应条件
hydrogenchloride
0.5 h;
参考文献
Abdullaeva,Kh.A. et al.
Chemistry of Natural Compounds, 1978 , vol. 14, p. 179 - 182
Khimiya Prirodnykh Soedinenii, 1978 , vol. 14, p. 219 - 223
参考文献
Boyd, Derek R.; Sharma, Narain D.; O'Dowd, Colin R.; Carroll, Jonathan G.; Loke, Pui L.; Allen, Christopher C. R.
Chemical Communications, 2005 , # 31 p. 3989 - 3991