(3-甲基丁-2-烯基)丙二酸二乙酯合成路线 （共 59 条）
反应条件
sodium hydride; Cl2Ni(1,2-bis(diphenylphosphino)ethane) in tetrahydrofuran
T=65°C; 36 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Alvarez, Eleuterio; Cuvigny, Therese; Julia, Marc
Journal of Organometallic Chemistry, 1988 , vol. 339, p. 199 - 212
反应条件
sodium hydride; Cl2Ni(1,2-bis(diphenylphosphino)ethane) in tetrahydrofuran
T=65°C; 36 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Alvarez, Eleuterio; Cuvigny, Therese; Julia, Marc
Journal of Organometallic Chemistry, 1988 , vol. 339, p. 199 - 212
反应条件
sodium hydride; Cl2Ni(1,2-bis(diphenylphosphino)ethane) in tetrahydrofuran
T=45°C; 36 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Alvarez, Eleuterio; Cuvigny, Therese; Julia, Marc
Journal of Organometallic Chemistry, 1988 , vol. 339, p. 199 - 212
反应条件
sodium hydride; bis-diphenylphosphinoethane; Pd(1,2-bis(diphenylphosphino)ethane)2 in tetrahydrofuran
36 h; Heating;
参考文献
Cuvigny, Therese; Julia, Marc; Rolando, C.
Journal of Organometallic Chemistry, 1985 , vol. 285, p. 395 - 414
反应条件
Cl2Ni(1,2-bis(diphenylphosphino)ethane) in tetrahydrofuran
T=65°C; 24 h; Yield given. Yields of byproduct given;
参考文献
Cuvigny, Therese; Julia, Marc
Journal of Organometallic Chemistry, 1983 , vol. 250, # 1 p. C21 - C24
反应条件
sodium hydride; bis-diphenylphosphinoethane; Pd(1,2-bis(diphenylphosphino)ethane)2 in tetrahydrofuran
36 h; Heating;
参考文献
Cuvigny, Therese; Julia, Marc; Rolando, C.
Journal of Organometallic Chemistry, 1985 , vol. 285, p. 395 - 414
反应条件
sodium hydride; bis-diphenylphosphinoethane; Pd(1,2-bis(diphenylphosphino)ethane)2 in tetrahydrofuran
36 h; Heating;
参考文献
Cuvigny, Therese; Julia, Marc; Rolando, C.
Journal of Organometallic Chemistry, 1985 , vol. 285, p. 395 - 414
反应条件
phenolated sodium; Pd(1,2-bis(diphenylphosphino)ethane)Cl2
T=135°C; 2 h; Further byproducts given;
参考文献
Cuvigny, Therese; Julia, Marc; Rolando, C.
Journal of Organometallic Chemistry, 1985 , vol. 285, p. 395 - 414
反应条件
triphenyl phosphite; sodium hydride; [Ir(μ-Cl)(1,5-cyclooctadiene)]2 in tetrahydrofuran
5 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Takeuchi; Kashio
Angewandte Chemie - International Edition in English, 1997 , vol. 36, # 3 p. 263 - 265
反应条件
1: pyridine / diethyl ether / Heating
2: 1.) NaH, 2.) Bu4N<Fe(CO)3NO> / 1.) THF, 10 min, 2.) THF, reflux, 12 h
View Scheme
参考文献
Xu, Yuanyao; Zhou, Bo
Journal of Organic Chemistry, 1987 , vol. 52, # 6 p. 974 - 977
