(3-甲基丁-2-烯基)丙二酸二乙酯合成路线 （共 59 条）
反应条件
1: 95 percent / LiCl, H2O / dimethylsulfoxide / 5 h / Heating 2: 56 percent / LiAlH4 / tetrahydrofuran View Scheme
参考文献
Cocker, Wesley; Geraghty, Niall W. A.; McMurry, T. Brian H.; Shannon, Patrick V. R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 10 p. 2245 - 2254
参考文献
Linstead; Rydon
Journal of the Chemical Society, 1933 , p. 583
反应条件
1: (i) KOH, EtOH, H2O, (ii) Cu, quinoline, (heating) 2: (COCl)2 / petroleum ether 3: diethyl ether 4: Cu / cyclohexane / Heating View Scheme
参考文献
Julia,S.; Linstrumelle,G.
Bulletin de la Societe Chimique de France, 1966 , p. 3490 - 3498
反应条件
1: durch Verseifung 2: Ueber mehreren Stufen 3: aqueous sulfuric acid View Scheme
参考文献
Linstead; Rydon
Journal of the Chemical Society, 1933 , p. 583
反应条件
hydrogen; palladium on activated charcoal in ethanol T=20°C;
参考文献
Kar, Paramita; Rao; Nagaiah; Gurjar
Journal of the Indian Chemical Society, 2005 , vol. 82, # 1 p. 52 - 54
反应条件
(i) NaOEt, EtOH, (ii) /BRN= 969135/; Multistep reaction;
参考文献
Julia,S.; Linstrumelle,G.
Bulletin de la Societe Chimique de France, 1966 , p. 3490 - 3498
反应条件
1: (i) KOH, EtOH, H2O, (ii) Cu, quinoline, (heating) 2: (COCl)2 / petroleum ether 3: diethyl ether View Scheme
参考文献
Julia,S.; Linstrumelle,G.
Bulletin de la Societe Chimique de France, 1966 , p. 3490 - 3498
参考文献
Becker; Haddad
Tetrahedron, 1993 , vol. 49, # 4 p. 947 - 964
反应条件
triethylaluminum; NiBr2(PPh3)2 in toluene
T=20°C; 24 h;
参考文献
Necas, David; Tursky, Matyas; Kotora, Martin
Journal of the American Chemical Society, 2004 , vol. 126, # 33 p. 10222 - 10223
反应条件
sodium hydride in tetrahydrofuran
1.) 0 deg C, 30 min; 2.) RT, 2 h;
参考文献
Cane, David E.; Tandon, Manish
Tetrahedron Letters, 1994 , vol. 35, # 30 p. 5355 - 5358
