2-氯-4-甲氧基-6-甲基嘧啶合成路线 （共 7 条）
反应条件
hydrogenchloride; sodium nitrite
参考文献
Yakugaku Zasshi, , vol. 73, p. 598,600
Chem.Abstr., , p. 9362
Bulletin des Societes Chimiques Belges, , vol. 68, p. 30,55
反应条件
1: methanol 2: aqueous NaNO2; aqueous HCl View Scheme
参考文献
Yakugaku Zasshi, , vol. 73, p. 598,600
Chem.Abstr., , p. 9362
参考文献
Bulletin des Societes Chimiques Belges, , vol. 68, p. 30,55
反应条件
in ethanol T=88°C; 6 h; stainless steel pressure vessel;
参考文献
Gershon; Grefig; Clarke
Journal of Heterocyclic Chemistry, 1987 , vol. 24, # 1 p. 205 - 209
反应条件
1: 60 percent / ethanol / 2.5 h / 88 °C
2: 62 percent / aq. 6N HCl / Heating; overnight
View Scheme
参考文献
Gershon, Herman; Grefig, Anthony T.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, p. 1161 - 1167
反应条件
1: 60 percent / ethanol / 2.5 h / 88 °C
2: 62 percent / aq. 6N HCl / Heating; overnight
3: 80 percent / phosphorus oxychloride / 3 h / Heating
View Scheme
参考文献
Gershon, Herman; Grefig, Anthony T.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, p. 1161 - 1167
反应条件
1: 64 percent / ethanol / 6 h / 88 °C / stainless steel pressure vessel
2: 80 percent / 6 N hydrochloric acid / Heating; overnight
View Scheme
参考文献
Gershon; Grefig; Clarke
Journal of Heterocyclic Chemistry, 1987 , vol. 24, # 1 p. 205 - 209
