3-(三氟甲基)苯甲酰氯合成路线 (共 34 条)
参考文献
Journal of the American Chemical Society, , vol. 70, p. 2837,2842
反应条件
1: carbon dioxide 2: thionyl chloride View Scheme
参考文献
Journal of the American Chemical Society, , vol. 70, p. 2837,2842
反应条件
1.1: sodium hydroxide / methanol / 20 °C 1.2: pH 2 2.1: thionyl chloride / dichloromethane / 2 h / 40 °C View Scheme
参考文献
WO2012/27965 A1, ;
WO 2012/027965 A1
反应条件
oxalyl dichloride in dichloromethane; N,N-dimethyl-formamide
参考文献
Journal of the American Chemical Society, , vol. 136, # 9 p. 3354 - 3357
反应条件
1: CHCl3 / Ambient temperature 2: 1M NaHCO3 / H2O / 17 h / Heating View Scheme
参考文献
Kane, John M.; Dudley, Mark W.; Sorensen, Stephen M.; Miller, Francis P.
Journal of Medicinal Chemistry, 1988 , vol. 31, # 6 p. 1253 - 1258
反应条件
triethylamine in dichloromethane T=20°C;
参考文献
Journal of Medicinal Chemistry, , vol. 51, # 8 p. 2400 - 2411
反应条件
water T=25°C; Rate constant;
参考文献
Campos-Rey; Cabaleiro-Lago; Herves
Journal of Physical Chemistry B, 2010 , vol. 114, # 44 p. 14004 - 14011
反应条件
hydrogenchloride; n-butyllithium; sodium hydrogencarbonate in tetrahydrofuran; hexane; ethyl acetate
参考文献
Nippon Shinyaku Co., Ltd.
Patent: US4711898 A1, 1987 ;
反应条件
quinoline; Pd-BaSO4; sulfur Hydrogenation.und Xylol;
参考文献
Lee, Sun-Hwa; Nikonov, Georgii I.
Dalton Transactions, 2014 , vol. 43, # 23 p. 8888 - 8893
反应条件
diethyl ether; dimethyl cadmium
参考文献
Corse et al.
Journal of the American Chemical Society, 1948 , vol. 70, p. 2837,2842