反应条件
1: 5-bromo-3-(4-chlorobut-2-enyl)-3-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecylsulfanyl)-6-methoxy-1,3-dihydroindol-2-one With samarium diiodide in tetrahydrofuran
T=20°C; 0.333333 h; Inert atmosphere;
2: Isopropyl(H)=NBn in tetrahydrofuran
T=80°C; Inert atmosphereSealed tube; diastereoselective reaction;
参考文献
Coote, Susannah C.; Quenum, Seidjolo; Procter, David J.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 14 p. 5104 - 5108