4-(4-硝基苯氧基)苯酚合成路线 （共 20 条）
反应条件
water; potassium carbonate; N,N-dimethyl-formamide T=135 - 140°C; 4.1 h; Yields of byproduct given;
参考文献
Dorogov; Derevyagin; Budanov; Plakhtinskii; Kotov
Russian Journal of Organic Chemistry, 1998 , vol. 34, # 5 p. 655 - 657
反应条件
1: 1.) KOH, 2.) CuCl / 1.) DMSO, RT, 5 min, 2.) DMSO, 70 deg C, 16 h 2: 91 percent / AlCl3, mercaptoethanol / C2H5SH / 3 h / 0 °C View Scheme
参考文献
Bao, Xiaofeng; Jin, Yanyan; Liu, Xiaolu; Liao, Hong; Zhang, Luyong; Pang, Tao
RSC Advances, 2014 , vol. 4, # 13 p. 6761 - 6775
反应条件
1: sodium hydride / N,N-dimethyl-formamide / 20 - 80 °C / Inert atmosphere 2: hydrogen bromide / 4 h / Inert atmosphere; Reflux View Scheme
参考文献
Li, Jie; Pei, Shuchen; Zhu, Yingxi; Wu, Jianbo; Chen, Yin; Zhang, Weiyu; Wu, Yong
Letters in Drug Design and Discovery, 2012 , vol. 9, # 4 p. 379 - 388
反应条件
water; potassium carbonate; hydroquinone
参考文献
Dorogov; Derevyagin; Budanov; Plakhtinskii; Kotov
Russian Journal of Organic Chemistry, 1998 , vol. 34, # 5 p. 655 - 657
反应条件
5 h; Heating; Mechanism;
参考文献
Iijima, Hiroyuki; Endo, Yasuyuki; Shudo, Koichi; Okamoto, Toshihiko
Tetrahedron, 1984 , vol. 40, # 23 p. 4981 - 4986
反应条件
potassium carbonate; potassium iodide in acetonitrile
Inert atmosphereReflux;
参考文献
Li, Jie; Pei, Shuchen; Zhu, Yingxi; Wu, Jianbo; Chen, Yin; Zhang, Weiyu; Wu, Yong
Letters in Drug Design and Discovery, 2012 , vol. 9, # 4 p. 379 - 388
反应条件
potassium carbonate; potassium iodide in acetonitrile
Inert atmosphereReflux;
参考文献
Li, Jie; Pei, Shuchen; Zhu, Yingxi; Wu, Jianbo; Chen, Yin; Zhang, Weiyu; Wu, Yong
Letters in Drug Design and Discovery, 2012 , vol. 9, # 4 p. 379 - 388
反应条件
1: 59 percent / K2CO3 / dimethylformamide / 50 °C
2: 72 percent / ammonium formate / 10 percent Pd/C / methanol / 20 °C
View Scheme
参考文献
Szurdoki; Szekacs; Le; Hammock
Journal of Agricultural and Food Chemistry, 2002 , vol. 50, # 1 p. 29 - 40
反应条件
1: potassium carbonate; potassium iodide / acetonitrile / Inert atmosphere; Reflux
2: stannous chloride-dihydrate; ethanol / 1 h / 70 °C / Inert atmosphere
View Scheme
参考文献
Li, Jie; Pei, Shuchen; Zhu, Yingxi; Wu, Jianbo; Chen, Yin; Zhang, Weiyu; Wu, Yong
Letters in Drug Design and Discovery, 2012 , vol. 9, # 4 p. 379 - 388
反应条件
1: potassium carbonate; potassium iodide / acetonitrile / Inert atmosphere; Reflux
2: stannous chloride-dihydrate; ethanol / 1 h / 70 °C / Inert atmosphere
View Scheme
参考文献
Li, Jie; Pei, Shuchen; Zhu, Yingxi; Wu, Jianbo; Chen, Yin; Zhang, Weiyu; Wu, Yong
Letters in Drug Design and Discovery, 2012 , vol. 9, # 4 p. 379 - 388
