3,7-二甲基辛-7-烯-1,6-二醇合成路线 （共 4 条）
反应条件
1: With sodium hydroxide; Na2MoO4 in methanol; water pH=11.7; 2: With dihydrogen peroxide in methanol; water T=55 - 73°C; 0.0833333 - 6 h; Conversion of starting material;
参考文献
Bourne, Richard A.; Han, Xue; Poliakoff, Martyn; George, Michael W.
Angewandte Chemie, International Edition, 2009 , vol. 48, # 29 p. 5322 - 5325
Angewandte Chemie, 2009 , vol. 121, # 29 p. 5426 - 5429
反应条件
triphenyl phosphite; ozone 1.) CH2Cl2, -80 deg C, 30 min; 2.) CH2Cl2, -80 deg C to room temp. then 2 h at room temp.; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Wahlen, Joos; De Vos, Dirk; Jary, Walther; Alsters, Paul; Jacobs, Pierre
Chemical Communications, 2007 , # 23 p. 2333 - 2335
反应条件
sodium tetrahydroborate in ethanol
参考文献
Shankaran,K.; Rao,A.S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1979 , vol. 18B, p. 507 - 509
反应条件
(i) O2, rose bengal, MeOH, (ii) H2SO4; Multistep reaction;
参考文献
Patel,J.S. et al.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1978 , vol. 16, p. 188 - 190
