1,3-二甲基-5-碘苯合成路线 （共 74 条）
反应条件
1,10-phenanthroline; oxygen; potassium iodide; copper(ll) bromide in N,N-dimethyl-formamide T=80°C; 20 h;
参考文献
Zhang, Guangyou; Lv, Guanglei; Li, Liping; Chen, Fan; Cheng, Jiang
Tetrahedron Letters, 2011 , vol. 52, # 16 p. 1993 - 1995
反应条件
copper(l) iodide; sodium iodide; N-methyl-2-(methylamino)ethylamine in 1,4-dioxane T=110°C; 20 h;
参考文献
Journal of Organic Chemistry, , vol. 70, # 17 p. 6904 - 6906
反应条件
1: With sulfuric acid; sodium nitrite in water; acetone T=0°C; 1.75 h; 2: With potassium iodide in water; acetone T=20°C;
参考文献
Xiang, Yanqiao; Caron, Pierre-Yves; Lillie, Brett M.; Vaidyanathan, Rajappa
Organic Process Research and Development, 2008 , vol. 12, # 1 p. 116 - 119
反应条件
copper(l) iodide; 1,10-phenanthroline; potassium iodide in methanol; water T=80°C; 1 h; High pressure;
参考文献
Partridge, Benjamin M.; Hartwig, John F.
Organic Letters, 2013 , vol. 15, # 1 p. 140 - 143
反应条件
iodine; silver trifluoroacetate in dichloromethane
参考文献
Journal of Labelled Compounds and Radiopharmaceuticals, , vol. 40, p. 65 - 67
反应条件
1: phenol With sodium hydride in tetrahydrofuran T=20°C; 0.5 h; Inert atmosphere; 2: With copper(l) chloride in tetrahydrofuran T=20°C; 0.5 h; Inert atmosphere; 3: 1,4-diiodo-2,6-dimethylbenzene Further stages;
参考文献
Angewandte Chemie - International Edition, , vol. 49, # 12 p. 2185 - 2189
反应条件
1: Diazotization; 2: iododediazotisation;
参考文献
Branchi, Barbara; Galli, Carlo; Gentili, Patrizia; Marinelli, Manuela; Mencarelli, Paolo
European Journal of Organic Chemistry, 2000 , # 14 p. 2663 - 2668
反应条件
1: Diazotization; 2: chlorodediazotisation;
参考文献
Branchi, Barbara; Galli, Carlo; Gentili, Patrizia; Marinelli, Manuela; Mencarelli, Paolo
European Journal of Organic Chemistry, 2000 , # 14 p. 2663 - 2668
反应条件
1: 70 percent / I2; Ag2SO4 View Scheme
参考文献
European Journal of Organic Chemistry, , # 14 p. 2663 - 2668
反应条件
copper(l) iodide; tributylphosphine; lithium tert-butylate in N,N-dimethyl-formamide T=60°C; 24 h; Inert atmosphere;
参考文献
Angewandte Chemie - International Edition, , vol. 51, # 2 p. 528 - 532
