雄甾-4-烯-3β,6β,17β-三醇合成路线 (共 40 条)
反应条件
tert.-butylhydroperoxide; dirhodium (II,II) caprolactamate in 1,2-dichloro-ethane T=40°C; Allylic oxidation; 16 h; Product distribution / selectivity;
参考文献
US2009/93638 A1, ;
Page/Page column 18-19 ;
反应条件
Montmorillonite K10; pyridinium chlorochromate in 1,4-dioxane 0.75 h; Irradiation;
参考文献
Tetrahedron, , vol. 55, # 11 p. 3255 - 3264
反应条件
tert.-butylhydroperoxide; dirhodium (II,II) caprolactamate in 1,2-dichloro-ethane T=40°C; Allylic oxidation; 16 h; Product distribution / selectivity;
参考文献
US2009/93638 A1, ;
Page/Page column 18-19 ;
反应条件
2-hydroxy-1,3-isoindolinedione; MeOAMVN; oxygen in acetonitrile T=30°C; P=760 Torr; 48 h;
参考文献
Synthetic Communications, , vol. 35, # 14 p. 1865 - 1874
反应条件
3 A molecular sieve; pyridinium chlorochromate in benzene 5 h; Heating;
参考文献
Synthetic Communications, , vol. 23, # 2 p. 223 - 230
反应条件
3-chloro-benzenecarboperoxoic acid in ethyl acetate 9 h; Ambient temperature;
参考文献
Journal of Chemical Research, Miniprint, , # 2 p. 718 - 734
反应条件
hydrogenchloride in dichloromethane 72 h; Ambient temperature;
参考文献
Journal of Chemical Research, Miniprint, , # 2 p. 718 - 734
反应条件
potassium tert-butylate in tert-butyl alcohol 20 h;
参考文献
Journal of Medicinal Chemistry, , vol. 28, # 6 p. 788 - 795
反应条件
tetrapropylammonium perruthennate; 4 A molecular sieve; 4-methylmorpholine N-oxide in dichloromethane T=25°C; ultrasonic irradiation; Yield given;
参考文献
Tetrahedron Letters, , vol. 32, # 27 p. 3201 - 3204
反应条件
pyridinium chlorochromate in dichloromethane 96 h;
参考文献
Synthetic Communications, , vol. 24, # 22 p. 3255 - 3259