5-苄氧基-2-硝基甲苯合成路线 (共 18 条)
反应条件
caesium carbonate in N,N-dimethyl-formamide T=20°C; 16 h;
参考文献
Wang, Yu-Yun; Chen, Chinpiao
Journal of Labelled Compounds and Radiopharmaceuticals, 2007 , vol. 50, # 14 p. 1262 - 1265
反应条件
potassium carbonate in N,N-dimethyl-formamide T=100°C; 1 h;
参考文献
Ohkubo, Mitsuru; Nishimura, Teruyuki; Jona, Hideki; Honma, Teruki; Morishima, Hajime
Tetrahedron, 1996 , vol. 52, # 24 p. 8099 - 8112
反应条件
sodium hydroxide; tetrabutylammomium bromide in hexane; dichloromethane; benzyl bromide
参考文献
Journal of the Chemical Society, , p. 402
反应条件
2,3-dimethylbutane-2,3-diol; [MoO2Cl2(dmf)2] in toluene T=150°C; 0.333333 h; Microwave irradiation;
参考文献
Garcia, Nuria; Garcia-Garcia, Patricia; Fernandez-Rodriguez, Manuel A.; Rubio, Ruben; Pedrosa, Maria R.; Arnaiz, Francisco J.; Sanz, Roberto
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 2-3 p. 321 - 327
反应条件
diethyl ether; potassium ethanolate
参考文献
Bergel; Morrison
Journal of the Chemical Society, 1943 , p. 49
Full Text Show Details
Burton; Stoves
Journal of the Chemical Society, 1937 , p. 402
参考文献
Bergel; Morrison
Journal of the Chemical Society, 1943 , p. 49
Full Text Show Details
Burton; Stoves
Journal of the Chemical Society, 1937 , p. 402
反应条件
1: 68 percent / dimethylformamide / 40 h / Heating 2: 100 percent / camphorsulfonic acid / 16 h / Heating 3: 70 percent / hydrogen / Pd/C / ethanol / 16 h / 20 °C View Scheme
参考文献
Todd, Matthew H.; Oliver, Steven F.; Abell, Chris
Organic Letters, 1999 , vol. 1, # 8 p. 1149 - 1151
反应条件
1: potassium ethylate; diethyl ether 2: FeSO4; aqueous NaOH 3: palladium/charcoal; methanol / Hydrogenation 4: copper-powder / 250 °C View Scheme
参考文献
Bergel; Morrison
Journal of the Chemical Society, 1943 , p. 49
反应条件
1: 2.) hydrazine hydrate / 2.) Raney nickel / 1.) reflux, 3 h, 2.) THF, MeOH, RT, 30 min 2: 1.) phosphorus oxychloride, 2.) conc. HCl / 1.) 0 deg C, 1 h, 2.) MeOH, THF, RT, 45 min View Scheme
参考文献
Buchheit; Gamse; Giger; Hoyer; Klein; Kloeppner; Pfannkuche; Mattes
Journal of medicinal chemistry, 1995 , vol. 38, # 13 p. 2331 - 2338