4-(5-溴-2-吡啶基)硫代吗啉合成路线 (共 2 条)
反应条件
sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium(0); 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in toluene T=98°C; 3 h; Inert atmosphere;
参考文献
IRM LLC; CHENG, Dai; ZHANG, Guobao; HAN, Dong; GAO, Wenqi; PAN, Shifeng
Patent: WO2010/101849 A1, 2010 ;
Location in patent: Page/Page column 108; 109 ;
WO 2010/101849 A1
参考文献
Endo, Hitoshi
Patent: EP1481965 A1, 2004 ;
Location in patent: Page 29 ;