7-氯-4,5-二氢-1H-苯并[b]氮杂革-2(3H)-酮合成路线 （共 6 条）
反应条件
chlorine in acetic acid 2.5 h; cold water bath;
参考文献
Chen; Gilman
Journal of Heterocyclic Chemistry, 1983 , vol. 20, # 3 p. 663 - 666
反应条件
1: 78.14 percent / polyphosphoric acid / 120 - 130 °C 2: 37.7 percent / sulfuryl chloride / benzene / 3 h / 20 °C View Scheme
参考文献
Ren, Hui; Zanger, Murray; McKee, James R.
Synthetic Communications, 2006 , vol. 36, # 3 p. 355 - 363
反应条件
1: 92.3 percent / hydroxylamine hydrochloride; pyridine / methanol / 2 h / Heating 2: 78.14 percent / polyphosphoric acid / 120 - 130 °C 3: 37.7 percent / sulfuryl chloride / benzene / 3 h / 20 °C View Scheme
参考文献
Ren, Hui; Zanger, Murray; McKee, James R.
Synthetic Communications, 2006 , vol. 36, # 3 p. 355 - 363
反应条件
1: reducing agent View Scheme
参考文献
Buege, Axel; Locke, Christian; Koehler, Thomas; Nuhn, Peter
Archiv der Pharmazie (Weinheim, Germany), 1994 , vol. 327, # 2 p. 99 - 104
参考文献
Buege, Axel; Locke, Christian; Koehler, Thomas; Nuhn, Peter
Archiv der Pharmazie (Weinheim, Germany), 1994 , vol. 327, # 2 p. 99 - 104
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 4 h; Heating;
参考文献
Ren, Hui; Zanger, Murray; McKee, James R.
Synthetic Communications, 2006 , vol. 36, # 3 p. 355 - 363
