(S)-(+)-1,2-异亚丙基甘油合成路线 (共 82 条)
反应条件
lithium hydroxide hydrate in tetrahydrofuran; water T=20°C; 12 h;
参考文献
European Journal of Organic Chemistry, , # 20 p. 4311 - 4318
反应条件
phosphate buffer; Lipase Amano PS in 1,4-dioxane T=30°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron Asymmetry, , vol. 8, # 6 p. 817 - 819
反应条件
phosphate buffer; Kluyveromyces marxianus CBS 4857 in water T=30°C; pH=7.0; 3 h; Title compound not separated from byproducts;
参考文献
Tetrahedron Asymmetry, , vol. 15, # 12 p. 1945 - 1947
反应条件
1: With ozone in dichloromethane T=-78°C; 1 h; oxygen atmosphere; 2: With sodium tetrahydroborate in ethanol; dichloromethane T=-78 - 50°C;
参考文献
Heterocycles, , vol. 76, # 2 p. 1285 - 1300
反应条件
Candida antarctica lipase B in ethyl acetate T=35°C; pH=7; 2 h; aq. phosphate bufferResolution of racemateEnzymatic reaction; optical yield given as percent ee;
参考文献
Journal of Molecular Catalysis B: Enzymatic, , vol. 69, # 1-2 p. 42 - 46
反应条件
Pseudomonas fluorecens Amano AK lipase in ethyl acetate T=30°C; pH=7; 5 h; aq. phosphate bufferResolution of racemateEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Journal of Molecular Catalysis B: Enzymatic, , vol. 69, # 1-2 p. 42 - 46
反应条件
Bacillus coagulans NCIMB 9365 dry cells in water; acetone T=25°C; pH=6.5; 7 h;
参考文献
Tetrahedron Asymmetry, , vol. 16, # 4 p. 841 - 845
反应条件
Bacillus coagulans NCIMB 9365 dry cells in water; acetone T=25°C; pH=6.5; 9 h;
参考文献
Tetrahedron Asymmetry, , vol. 16, # 4 p. 841 - 845
反应条件
Bacillus coagulans NCIMB 9365 dry cells in water; acetone T=25°C; pH=6.5; 8 h;
参考文献
Tetrahedron Asymmetry, , vol. 16, # 4 p. 841 - 845
反应条件
magnesium chloride; alkaline phosphatase in water 24 h; Yield given;
参考文献
Journal of Organic Chemistry, , vol. 63, # 12 p. 4039 - 4045