1,3-二(甲苯磺酰氧基)-2,2-二甲基丙烷合成路线 (共 12 条)
反应条件
1: 195 °C
2: aq. KOH / Heating
View Scheme
参考文献
Brown,H.C. et al.
Journal of the American Chemical Society, 1977 , vol. 99, # 2 p. 505 - 509
反应条件
1: 71 percent / ethane-1,2-diol / 2 h / Heating
2: 85 percent / NaOH / H2O / 48 h / Heating
3: 89 percent / Thionyl chloride
View Scheme
参考文献
Wills, Max T.; Wills, Irene E.; Dollen, Lawrence Von; Butler, Barry L.; Porter, John; Anderson, Arthur G.
Journal of Organic Chemistry, 1980 , vol. 45, # 12 p. 2489 - 2498