(E)-3-(4-甲氧基苯基)-1-苯基-丙-2-烯-1-酮合成路线 (共 63 条)
反应条件
1: With potassium tert-butylate in tetrahydrofuran
T=-78°C; 0.166667 h;
2: With sulfuric acid in ethylene glycol dimethyl ether
T=-78°C; 0.166667 h;
参考文献
Yoshizawa, Kazuhiro; Shioiri, Takayuki
Tetrahedron Letters, 2006 , vol. 47, # 28 p. 4943 - 4945
反应条件
1: 4-methoxy-benzaldehyde With sodium ethanolate in toluene
T=25°C; 0.25 h; Inert atmosphere;
2: (2-Oxo-2-phenylethyl)triphenylphosphonium bromide in toluene
T=80°C; Wittig reaction; 6 h;
参考文献
Bera, Rabin; Dhananjaya; Singh, Shambu Nath; Kumar, Rajender; Mukkanti; Pal, Manojit
Tetrahedron, 2009 , vol. 65, # 7 p. 1300 - 1305
反应条件
palladium diacetate; copper (II) acetate monohydrate; potassium carbonate in N,N-dimethyl-formamide
T=120°C; Inert atmosphere;
参考文献
Unoh, Yuto; Hirano, Koji; Satoh, Tetsuya; Miura, Masahiro
Journal of Organic Chemistry, 2013 , vol. 78, # 10 p. 5096 - 5102
反应条件
tin tetraiodide; tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine in dichloromethane
T=-80°C; 48 h;
参考文献
Masuyama, Yoshiro; Ohtsuka, Masaru; Kondo, Ayako
Synlett, 2006 , # 19 p. 3346 - 3348
反应条件
in dimethyl sulfoxide
T=100°C; 12 h; Inert atmosphere; optical yield given as percent destereoselective reaction;
参考文献
Fang, Fan; Li, Yuan; Tian, Shi-Kai
European Journal of Organic Chemistry, 2011 , # 6 p. 1084 - 1091
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in tetrahydrofuran
Julia-Kocienski olefination; optical yield given as percent destereoselective reaction;
参考文献
Kumar, Atul; Sharma, Siddharth; Tripathi, Vishwa Deepak; Srivastava, Suman
Tetrahedron, 2010 , vol. 66, # 48 p. 9445 - 9449
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in tetrahydrofuran
Julia-Kocienski olefination; optical yield given as percent destereoselective reaction;
参考文献
Kumar, Atul; Sharma, Siddharth; Tripathi, Vishwa Deepak; Srivastava, Suman
Tetrahedron, 2010 , vol. 66, # 48 p. 9445 - 9449
反应条件
indium monobromide in tetrahydrofuran
14 h; Heating;
参考文献
Peppe, Clovis; das Chagas, Rafael Pavao
Journal of Organometallic Chemistry, 2006 , vol. 691, # 26 p. 5868 - 5872
反应条件
sodium hydride in ethylene glycol dimethyl ether
7 h; Heating;
参考文献
Liguori, Angelo; Romeo, Giovanni; Sindona, Giovanni; Uccella, Nicola
Gazzetta Chimica Italiana, 1991 , vol. 121, # 8 p. 393 - 395
反应条件
silica gel
0.1 h; Irradiation;
参考文献
Xu, Caiding; Chen, Guoying; Huang, Xian
Organic Preparations and Procedures International, 1995 , vol. 27, # 5 p. 559 - 561