反应条件
1: 1.) Li, n-BuLi / 1.) ether, 2 h, room temperature, 2.) a) 45 min, salt-ice bath, b) 15 min, room temperature
2: 95 percent / methyl sulfide, N-chlorosuccinimide / toluene; CH2Cl2 / 2 h / -25 °C
3: 81 percent / AgNO3, 5 N aqueous NaOH / ethanol / 4 h / Ambient temperature
View Scheme
参考文献
Sahali, Y.; Skipper, P. L.; Tannenbaum, S. R.
Journal of Organic Chemistry, 1990 , vol. 55, # 9 p. 2918 - 2920
