(S)-4-甲基唑烷-2,5-二酮合成路线 (共 22 条)
反应条件
carbon in tetrahydrofuran T=55°C; 1.5 h;
参考文献
Journal of Organic Chemistry, , vol. 50, # 5 p. 715 - 716
反应条件
N,N-dimethyl-formamide in dichloromethane T=0 - 20°C;
参考文献
Journal of Organic Chemistry, , vol. 50, # 12 p. 2200 - 2202
反应条件
N,N-dimethyl-formamide in dichloromethane T=0°C; 1 h;
参考文献
Journal of the American Chemical Society, , vol. 120, # 41 p. 10646 - 10652
反应条件
phosphorus trichoride in dichloromethane T=0°C; 2 h;
参考文献
Tetrahedron, , vol. 50, # 30 p. 9051 - 9060
反应条件
in tetrahydrofuran T=30°C; 3.5 h;
参考文献
Journal of Organic Chemistry, , vol. 53, # 4 p. 836 - 844
反应条件
in tetrahydrofuran 2 h; Inert atmosphere;
参考文献
Journal of Polymer Science, Part A: Polymer Chemistry, , vol. 50, # 6 p. 1076 - 1085
反应条件
bis(trichloromethyl) carbonate in tetrahydrofuran T=50°C; 3 - 4 h;
参考文献
US2005/276783 A1, ;
Page/Page column 6 ;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1317 - 1324
反应条件
phosphorus tribromide in diethyl ether
参考文献
Journal of Organic Chemistry, , vol. 57, # 28 p. 7334 - 7338