2,3,4,5,6-五溴硝基苯合成路线 （共 12 条）
反应条件
sulfuric acid; bromine; mercury(II) oxide T=47°C; 1.3 h;
参考文献
Shishkin, V.N.; Bolusheva, I.Yu.; Lapin, K.K.; Tanaseichuk, B.S.
Journal of Organic Chemistry USSR (English Translation), 1991 , vol. 27, # 7 p. 1303 - 1308
Zhurnal Organicheskoi Khimii, 1991 , vol. 27, # 7 p. 1486 - 1492
反应条件
sulfuric acid; bromine; nitric acid T=80 - 85°C;
参考文献
Andrievskii, A.M.; Gorelik, M.V.; Avidon, S.V.; Al'tman, E.Sh.
Russian Journal of Organic Chemistry, 1993 , vol. 29, # 9.2 p. 1519 - 1524
Zhurnal Organicheskoi Khimii, 1993 , vol. 29, # 9 p. 1828 - 1834
参考文献
Qvist
Acta Academiae Aboensis, Series B: Mathematica et Physica, 1936 , vol. 10, # 5 p. 3,27
反应条件
sulfuric acid; bromine; mercury(II) oxide T=47 - 50°C; 1.3 h; Yield given. Yields of byproduct given;
参考文献
Shishkin, V.N.; Bolusheva, I.Yu.; Lapin, K.K.; Tanaseichuk, B.S.
Journal of Organic Chemistry USSR (English Translation), 1991 , vol. 27, # 7 p. 1303 - 1308
Zhurnal Organicheskoi Khimii, 1991 , vol. 27, # 7 p. 1486 - 1492
参考文献
Jacobson; Loeb
Chemische Berichte, 1900 , vol. 33, p. 705
Full Text Show Details
Jackson; Bancroft
American Chemical Journal, 1890 , vol. 12, p. 294
反应条件
1: aqueous H2SO4 / Diazotization.Behandlung der Diazoniumsalz-Loesung mit KBr und Brom und Erhitzen des gebildeten Perbromids in Eisessig auf dem Dampfbad 2: fuming nitric acid View Scheme
参考文献
Qvist
Acta Academiae Aboensis, Series B: Mathematica et Physica, 1949 , vol. 17, # 6 p. 3,10
反应条件
sulfuric acid; bromine; nitric acid 3 h;
参考文献
Andrievskii, A.M.; Gorelik, M.V.; Avidon, S.V.; Al'tman, E.Sh.
Russian Journal of Organic Chemistry, 1993 , vol. 29, # 9.2 p. 1519 - 1524
Zhurnal Organicheskoi Khimii, 1993 , vol. 29, # 9 p. 1828 - 1834
反应条件
(i) Hg(O2CCF3)2, (ii) KBr3, aq. MeOH; Multistep reaction;
参考文献
Deacon,G.B.; Farquharson,G.J.
Australian Journal of Chemistry, 1977 , vol. 30, p. 293 - 304
反应条件
in benzene T=340°C; in sealed tube; other solvent (neat); other temp.; Product distributionKineticsRate constant;
参考文献
Oxley, Jimmie C.; Smith, James L.; Ye, Hong; McKenney, Robert L.; Bolduc, Paul R.
Journal of Physical Chemistry, 1995 , vol. 99, # 23 p. 9593 - 9602
参考文献
Qvist
Acta Academiae Aboensis, Series B: Mathematica et Physica, 1936 , vol. 10, # 5 p. 3,27
