4-碘-N,N-二甲基苯磺胺合成路线 （共 4 条）
反应条件
4-(N,N-dimethlyamino)pyridine; dimethyl amine in tetrahydrofuran; pyridine; water; ethyl acetate
参考文献
Chang, Kwen-Jen; King, Klim; Biciunas, Kestutis P.; McNutt JR., Robert W.; Pendergast, William; Jan, Shyi-Tai
Patent: US2003/186872 A1, 2003 ;
参考文献
Debergh, J. Robb; Niljianskul, Nootaree; Buchwald, Stephen L.
Journal of the American Chemical Society, 2013 , vol. 135, # 29 p. 10638 - 10641
反应条件
1: phenyl sulphuryl chloride; sodium carbonate; C43H43NO3PPdS / acetone / 12 h / 55 °C / |Inert atmosphere; |Sealed tube 2: tetrahydrofuran / 0 - 20 °C / |Inert atmosphere View Scheme
参考文献
Debergh, J. Robb; Niljianskul, Nootaree; Buchwald, Stephen L.
Journal of the American Chemical Society, 2013 , vol. 135, # 29 p. 10638 - 10641
反应条件
potassium acetate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct in dimethyl sulfoxide T=80°C; 17 h;
参考文献
WO2006/4703 A2, ;
Page/Page column 37-38 ;
WO 2006/004703 A2
